Octahydro-6,7a-dimethyl-2-oxo-3,6-methanobenzofuran-4,5,8-tricarboxylic acid trimethyl ester

Base Information

• Chemical Name: Octahydro-6,7a-dimethyl-2-oxo-3,6-methanobenzofuran-4,5,8-tricarboxylic acid trimethyl ester
• CAS No.: 32251-36-8
• Molecular Formula: C₁₇H₂₂O₈
• Molecular Weight: 354.357
• Mol file: 32251-36-8.mol

Synonyms:Octahydro-6,7a-dimethyl-2-oxo-3,6-methanobenzofuran-4,5,8-tricarboxylic acid trimethyl ester

Chemical Property of Octahydro-6,7a-dimethyl-2-oxo-3,6-methanobenzofuran-4,5,8-tricarboxylic acid trimethyl ester

Chemical Property:

• Melting Point: 155 °C
• PSA: 105.20000
• LogP: 0.32550

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Octahydro-6,7a-dimethyl-2-oxo-3,6-methanobenzofuran-4,5,8-tricarboxylic acid trimethyl ester

There total 3 articles about Octahydro-6,7a-dimethyl-2-oxo-3,6-methanobenzofuran-4,5,8-tricarboxylic acid trimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 7-hydroxy-4,7-dimethyl-bicyclo[2.2.2]octane-2exo,3exo,5exo,6exo-tetracarboxylic acid-2-lactone-3,5,6-trimethyl ester (32251-36-8)

Guidance literature:

With water; Behandeln des Reaktionsprodukts mit Diazomethan in Aether;

Reference yield:

water (7732-18-5) + 1,14-dimethyl-4,10-dioxatetracyclo[5.5.2.02,608,12]tetradec-13-ene-3,5,9,11-tetraone (32251-35-7,134932-59-5) → 7-hydroxy-4,7-dimethyl-bicyclo[2.2.2]octane-2exo,3exo,5exo,6exo-tetracarboxylic acid-2-lactone-3,5,6-trimethyl ester (32251-36-8)

Guidance literature:

Behandeln des Reaktionsprodukts mit Diazomethan in Aether;

DOI:10.1021/jo00966a033

Reference yield:

→ (6R,7R,8S,9S,10R)-1,3-Dimethyl-5-oxo-4-oxa-tricyclo[4.3.1.03,7]decane-8,9,10-tricarboxylic acid trimethyl ester (32251-36-8)

Guidance literature:

aus dem Dianhydrid 4, 1) NaHCO3-Lsg., 2) HCl, 3) CH2N2;

DOI:10.1021/jo00966a033

upstream raw materials:

water

1,14-dimethyl-4,10-dioxatetracyclo[5.5.2.0^2,60^8,12]tetradec-13-ene-3,5,9,11-tetraone

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