5-(2-METHOXYPHENYL)-3-ISOXAZOLEMETHANOL

Base Information

• Chemical Name: 5-(2-METHOXYPHENYL)-3-ISOXAZOLEMETHANOL
• CAS No.: 110578-29-5
• Molecular Formula: C11H11NO3
• Molecular Weight: 205.213
• Mol file: 110578-29-5.mol

Synonyms:5-(2-METHOXYPHENYL)-3-ISOXAZOLEMETHANOL

Chemical Property of 5-(2-METHOXYPHENYL)-3-ISOXAZOLEMETHANOL

Chemical Property:

• Melting Point: 90-91 °C
• Boiling Point: 354.3±32.0 °C(Predicted)
• PKA: 13.02±0.10(Predicted)
• PSA: 55.49000
• Density: 1.217±0.06 g/cm3(Predicted)
• LogP: 1.84250

Purity/Quality:

5-(2-METHOXYPHENYL)-3-ISOXAZOLEMETHANOL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 5-(2-METHOXYPHENYL)-3-ISOXAZOLEMETHANOL

There total 1 articles about 5-(2-METHOXYPHENYL)-3-ISOXAZOLEMETHANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(2-methoxyphenyl)isoxazole-3-carboxylic acid methyl ester (668971-17-3) → [5-(2-Methoxy-phenyl)-isoxazol-3-yl]-methanol (110578-29-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran;

DOI:10.3390/molecules21121722

Reference yield: 82.0%

[5-(2-Methoxy-phenyl)-isoxazol-3-yl]-methanol (110578-29-5) → 2-buten-1-one-3-amino-4-hydroxy-1-o-methoxyphenyl (110578-34-2)

Guidance literature:

With hydrogen; platinum(IV) oxide; nickel; In ethanol; under 760 Torr; Ambient temperature;

DOI:10.1016/S0040-4020(01)89949-X

Reference yield:

[5-(2-Methoxy-phenyl)-isoxazol-3-yl]-methanol (110578-29-5) → C10H8NOClCH2O

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane; at 45 ℃; for 8h;

DOI:10.3390/molecules21121722

upstream raw materials:

5-(2-methoxyphenyl)isoxazole-3-carboxylic acid methyl ester

Downstream raw materials:

2-buten-1-one-3-amino-4-hydroxy-1-o-methoxyphenyl

5-o-methoxyphenyl-3(2H)-furanone

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