α-(4-Hydroxyimino-3-methyl-2,5-cyclohexadien-1-ylidene)-4-methoxybenzeneacetonitrile

Base Information

Chemical Name:α-(4-Hydroxyimino-3-methyl-2,5-cyclohexadien-1-ylidene)-4-methoxybenzeneacetonitrile
CAS No.:7380-63-4
Molecular Formula:C₁₈H₂₆N₂O₁₀
Molecular Weight:430.412
Hs Code.:

Synonyms:α-(4-Hydroxyimino-3-methyl-2,5-cyclohexadien-1-ylidene)-4-methoxybenzeneacetonitrile

Suppliers and Price of α-(4-Hydroxyimino-3-methyl-2,5-cyclohexadien-1-ylidene)-4-methoxybenzeneacetonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of α-(4-Hydroxyimino-3-methyl-2,5-cyclohexadien-1-ylidene)-4-methoxybenzeneacetonitrile

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

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Technology Process of α-(4-Hydroxyimino-3-methyl-2,5-cyclohexadien-1-ylidene)-4-methoxybenzeneacetonitrile

There total 11 articles about α-(4-Hydroxyimino-3-methyl-2,5-cyclohexadien-1-ylidene)-4-methoxybenzeneacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80681-54-5,80735-45-1
Acetic acid (3S,4R,5R,6S)-5-acetylamino-3,4-dihydroxy-6-methoxy-tetrahydro-pyran-2-yl ester

: 7380-63-4
hexaacetyl-streptamine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) MeOH-H₂O= 2:1 2.) 10 percent NaOMe(MeOH) / 1.) 17 deg C, 10 min, 2.) MeOH, H₂O, 48 h, 17 deg C

2: H₂ / Raney Ni(T-4) / ethanol; H₂O / 6 h

3: pyridine / 12 h / 18 °C

With pyridine; methanol; water; hydrogen; sodium methylate; Raney Ni(T-4); In ethanol; water;
DOI:10.1248/cpb.29.2582

Reference yield:

: 561307-75-3
N-((1S,2R,3S,4S,5R,6S)-2,3,4,6-Tetrahydroxy-5-nitro-cyclohexyl)-acetamide

: 7380-63-4
hexaacetyl-streptamine

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Raney Ni(T-4) / ethanol; H₂O / 6 h

2: pyridine / 12 h / 18 °C

With pyridine; hydrogen; Raney Ni(T-4); In ethanol; water;
DOI:10.1248/cpb.29.2582

Reference yield:

: N-[(1S,2S,3R,4S,5R,6R)-2,4-Dihydroxy-5,6-bis-(2-methoxy-ethoxymethoxy)-3-nitro-cyclohexyl]-acetamide

: 7380-63-4
hexaacetyl-streptamine

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Raney Ni(T-4) / ethanol / 6 h / Ambient temperature

2: pyridine

3: TiCl₄ / CH₂Cl₂ / 16 h / 19 °C

4: pyridine

With pyridine; hydrogen; titanium tetrachloride; Raney Ni(T-4); In ethanol; dichloromethane;
DOI:10.1248/cpb.29.2582