N-[(1S)-2'-aMino[1,1'-binaphthalen]-2-yl]-4-Methyl-BenzenesulfonaMide

Base Information

Chemical Name:N-[(1S)-2'-aMino[1,1'-binaphthalen]-2-yl]-4-Methyl-BenzenesulfonaMide
CAS No.:933782-32-2
Molecular Formula:C₂₇H₂₂N₂O₂S
Molecular Weight:438.55
Hs Code.:
Mol file:933782-32-2.mol

Synonyms:N-[(1S)-2'-aMino[1,1'-binaphthalen]-2-yl]-4-Methyl-BenzenesulfonaMide;[(S)-N-2'-Amino[1,1'-binaphthalen]-2-yl]-4-methylbenzenesulfonamide;N-[(S)-2'-Amino-[1,1'-binaphthalen]-2-yl]-4- methylbenzenesulfonamide

Suppliers and Price of N-[(1S)-2'-aMino[1,1'-binaphthalen]-2-yl]-4-Methyl-BenzenesulfonaMide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 7 raw suppliers

Chemical Property of N-[(1S)-2'-aMino[1,1'-binaphthalen]-2-yl]-4-Methyl-BenzenesulfonaMide

Chemical Property:

Boiling Point:632.9±65.0 °C (760 mmHg)
PSA：80.57000
Density:1.326±0.06 g/cm3 (20 °C, 760 mmHg)
LogP:8.08640

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-[(1S)-2'-aMino[1,1'-binaphthalen]-2-yl]-4-Methyl-BenzenesulfonaMide

There total 1 articles about N-[(1S)-2'-aMino[1,1'-binaphthalen]-2-yl]-4-Methyl-BenzenesulfonaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 4488-22-6,18531-95-8
1,1'-binaphthalene-2,2'-diamine

: 98-59-9
p-toluenesulfonyl chloride

: 933782-32-2,512170-32-0,903550-11-8
N-(2'-amino-[1,1'-binaphthalen]-2-yl)-4-methylbenzenesulfonamide

Guidance literature:: With pyridine; In acetonitrile; for 12h; Reflux; Inert atmosphere;
DOI:10.1016/j.tetlet.2015.12.008

Reference yield: 72.0%

: 933782-32-2,512170-32-0,903550-11-8
N-(2'-amino-[1,1'-binaphthalen]-2-yl)-4-methylbenzenesulfonamide

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 131543-46-9,107-22-2
Glyoxal

: 902777-94-0
2-(tosylamino)-2'-(imidazol-1-yl)-1,1'-binaphthyl

Guidance literature:: With phosphoric acid; ammonium chloride; In 1,4-dioxane; water; for 6h; Heating;
DOI:10.1016/j.tet.2006.04.034

Reference yield: 49.0%

: 933782-32-2,512170-32-0,903550-11-8
N-(2'-amino-[1,1'-binaphthalen]-2-yl)-4-methylbenzenesulfonamide

: 2449-05-0
dibenzyl azodicarboxylate

: (S_a)-N-[2-amino-(1,1'-binaphthyl)-2-yl]-4-methylbenzenesulfonamide

: (R)-dibenzyl 3-(2'-((4-methylphenyl)sulfonamido)-[1,1'-binaphthalen]-2-yl)triazane-1,2-dicarboxylate

Guidance literature:: With (R)-TRIP; In chloroform; at -40 ℃; for 0.6h; enantioselective reaction; Catalytic behavior; Resolution of racemate;