(4bS,8aβ,9β)-4b,5,6,7,8,8a,9,10-Octahydro-1,3,4-trimethoxy-4bα,8,8-trimethyl-2-isopropyl-9-phenanthrenol

Base Information

Chemical Name:(4bS,8aβ,9β)-4b,5,6,7,8,8a,9,10-Octahydro-1,3,4-trimethoxy-4bα,8,8-trimethyl-2-isopropyl-9-phenanthrenol
CAS No.:60371-75-7
Molecular Formula:
Molecular Weight:376.53
Hs Code.:
Mol file:60371-75-7.mol

Synonyms:9-Phenanthrenol, 4b,5,6,7,8,8a,9,10-octahydro-1,3,4-trimethoxy-4b,8,8-trimethyl-2-(1-methylethyl)-, [4bS-(4bα,8aβ,9β)]- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4bS,8aβ,9β)-4b,5,6,7,8,8a,9,10-Octahydro-1,3,4-trimethoxy-4bα,8,8-trimethyl-2-isopropyl-9-phenanthrenol

Chemical Property:

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Safty Information:

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Useful:

Technology Process of (4bS,8aβ,9β)-4b,5,6,7,8,8a,9,10-Octahydro-1,3,4-trimethoxy-4bα,8,8-trimethyl-2-isopropyl-9-phenanthrenol

There total 5 articles about (4bS,8aβ,9β)-4b,5,6,7,8,8a,9,10-Octahydro-1,3,4-trimethoxy-4bα,8,8-trimethyl-2-isopropyl-9-phenanthrenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 60371-72-4,130852-89-0,130852-90-3
(4bR,8aR)-2-Isopropyl-1,3,4-trimethoxy-4b,8,8-trimethyl-4b,6,7,8,8a,10-hexahydro-5H-phenanthren-9-one

: 60371-73-5,60371-75-7,130741-01-4,130852-91-4
(4bR,8aR)-2-Isopropyl-1,3,4-trimethoxy-4b,8,8-trimethyl-4b,5,6,7,8,8a,9,10-octahydro-phenanthren-9-ol

Guidance literature:: With lithium aluminium tetrahydride;
DOI:10.1016/S0040-4039(00)97454-9

Reference yield:

: 60371-72-4
11,12,14-Trimethoxy-abieta-8,11,13-trien-6-on

: 60371-73-5
11,12,14-Trimethoxy-abieta-8,11,13-trien-6β-ol

: 60371-75-7
11,12,14-Trimethoxy-abieta-8,11,13-trien-6α-ol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; Heating;

Reference yield:

: 130741-00-3
2-(3-Isopropyl-2,4,5-trimethoxy-phenyl)-1-(2,6,6-trimethyl-cyclohex-1-enyl)-ethanone

: 60371-73-5,60371-75-7,130741-01-4,130852-91-4
(4bR,8aR)-2-Isopropyl-1,3,4-trimethoxy-4b,8,8-trimethyl-4b,5,6,7,8,8a,9,10-octahydro-phenanthren-9-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 29 percent / TFA / 24 h / Heating

2: 90 percent / LiAlH₄

With lithium aluminium tetrahydride; trifluoroacetic acid;
DOI:10.1016/S0040-4039(00)97454-9