5-Bromo-2-methoxybenzamide

Base Information

Chemical Name:5-Bromo-2-methoxybenzamide
CAS No.:303111-31-1
Molecular Formula:C8H8BrNO2
Molecular Weight:230.061
Hs Code.:2924299090
DSSTox Substance ID:DTXSID60589280
Nikkaji Number:J1.387.811K
Wikidata:Q82482541
Mol file:303111-31-1.mol

Synonyms:5-bromo-2-methoxybenzamide;303111-31-1;benzamide, 5-bromo-2-methoxy-;CHEMBRDG-BB 9027573;SCHEMBL9621997;DTXSID60589280;MFCD08105424;STL503440;AKOS000299481;MCULE-4155621328;SB77316;DA-37822;LS-03763;CS-0212853;W18958

Suppliers and Price of 5-Bromo-2-methoxybenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-Bromo-2-methoxybenzamide
1g
$ 240.00

Crysdot
5-Bromo-2-methoxybenzamide 95+%
5g
$ 414.00

Chemcia Scientific
5-Bromo-2-methoxy-benzamide 95%
5 G
$ 415.00

ChemBridge Corporation
5-bromo-2-methoxybenzamide 95%
250 mg
$ 64.00

Biosynth Carbosynth
5-Bromo-2-methoxybenzamide
1 g
$ 340.00

Biosynth Carbosynth
5-Bromo-2-methoxybenzamide
250 mg
$ 130.00

Biosynth Carbosynth
5-Bromo-2-methoxybenzamide
100 mg
$ 65.00

Biosynth Carbosynth
5-Bromo-2-methoxybenzamide
500 mg
$ 210.00

Biosynth Carbosynth
5-Bromo-2-methoxybenzamide
2 g
$ 490.00

American Custom Chemicals Corporation
5-BROMO-2-METHOXYBENZAMIDE 95.00%
5MG
$ 505.74

Total 5 raw suppliers

Chemical Property of 5-Bromo-2-methoxybenzamide

Chemical Property:

Vapor Pressure:0.001mmHg at 25°C
Boiling Point:304.02°C at 760 mmHg
PKA:14.97±0.50(Predicted)
Flash Point:137.667°C
PSA：52.32000
Density:1.551g/cm³
LogP:2.25690
XLogP3:2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:228.97384
Heavy Atom Count:12
Complexity:174

Purity/Quality:

98%min ^*data from raw suppliers

5-Bromo-2-methoxybenzamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)Br)C(=O)N

Technology Process of 5-Bromo-2-methoxybenzamide

There total 4 articles about 5-Bromo-2-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16740-73-1
5-bromo-2-methoxyacetophenone

: 303111-31-1
2-methoxy-5-bromobenzene carboxamide

Guidance literature:: With ammonium hydroxide; iodine; In acetonitrile; at 60 ℃; for 12h;
DOI:10.1021/acs.orglett.6b00048

Reference yield:

: 14804-32-1
2-ethylanisole

: 303111-31-1
2-methoxy-5-bromobenzene carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); water / chloroform / 18 h / 60 °C

2: ammonium hydroxide; iodine / acetonitrile / 12 h / 60 °C

With ammonium hydroxide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); water; iodine; In chloroform; acetonitrile;
DOI:10.1021/acs.orglett.6b00048