4-Aminobenzoic (2-chlorobenzylidene)hydrazide

Base Information

• Chemical Name: 4-Aminobenzoic (2-chlorobenzylidene)hydrazide
• CAS No.: 35559-01-4
• Molecular Formula: C₁₄H₁₂ClN₃O
• Molecular Weight: 273.722
• European Community (EC) Number: 668-666-0
• Mol file: 35559-01-4.mol

Synonyms:AKOS003665194;SR-01000209841;SR-01000209841-1;4-AMINOBENZOIC (2-CHLOROBENZYLIDENE)HYDRAZIDE

Chemical Property of 4-Aminobenzoic (2-chlorobenzylidene)hydrazide

Chemical Property:

• XLogP3: 2.5
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 273.0668897
• Heavy Atom Count: 19
• Complexity: 327

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)C=NNC(=O)C2=CC=C(C=C2)N)Cl
• Isomeric SMILES: C1=CC=C(C(=C1)/C=N/NC(=O)C2=CC=C(C=C2)N)Cl

Technology Process of 4-Aminobenzoic (2-chlorobenzylidene)hydrazide

There total 1 articles about 4-Aminobenzoic (2-chlorobenzylidene)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2-chloro-benzaldehyde (89-98-5) + 4-aminobenzohydrazide (5351-17-7) → 4-Amino-benzoic acid [1-(2-chloro-phenyl)-meth-(E)-ylidene]-hydrazide (35559-01-4)

Guidance literature:

In ethanol;

Reference yield: 81.0%

4-Amino-benzoic acid [1-(2-chloro-phenyl)-meth-(E)-ylidene]-hydrazide (35559-01-4) + phenyl isothiocyanate (103-72-0) → 1-{4-[1-(2-Chloro-phenyl)-meth-(E)-ylidene-hydrazinocarbonyl]-phenyl}-3-phenyl-thiourea

Guidance literature:

In 1,4-dioxane;

Reference yield:

indole (120-72-9) + 4-Amino-benzoic acid [1-(2-chloro-phenyl)-meth-(E)-ylidene]-hydrazide (35559-01-4) → 4-(1H-Indol-3-ylazo)-benzoic acid [1-(2-chloro-phenyl)-meth-(E)-ylidene]-hydrazide (132256-01-0)

Guidance literature:

With hydrogenchloride; potassium hydroxide; sodium nitrite; Yield given. Multistep reaction; 1) 0 deg C;

upstream raw materials:

2-chloro-benzaldehyde

4-aminobenzohydrazide

Downstream raw materials:

4-(1H-Indol-3-ylazo)-benzoic acid [1-(2-chloro-phenyl)-meth-(E)-ylidene]-hydrazide

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