N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-O-(2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl)-L-serine pentafluorophenyl ester

Base Information

• Chemical Name: N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-O-(2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl)-L-serine pentafluorophenyl ester
• CAS No.: 478062-63-4
• Molecular Formula: C38H34F5NO14
• Molecular Weight: 0
• Mol file: 478062-63-4.mol

Synonyms:N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-O-(2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl)-L-serine pentafluorophenyl ester

Chemical Property of N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-O-(2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl)-L-serine pentafluorophenyl ester

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

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MSDS Files:

SDS file from LookChem

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Technology Process of N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-O-(2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl)-L-serine pentafluorophenyl ester

There total 2 articles about N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-O-(2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl)-L-serine pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

D-glucose pentaacetate (83-87-4,604-68-2,604-69-3,2152-77-4,4026-35-1,4163-59-1,4163-60-4,4163-61-5,4163-65-9,4257-94-7,4257-96-9,16299-15-3,19186-39-1,19189-55-0,25878-60-8,25941-03-1,32445-48-0,32445-49-1,32445-53-7,32445-54-8,34685-58-0,34685-59-1,43168-42-9,43168-44-1,43169-22-8,43169-25-1,66966-07-2,70749-17-6,80184-01-6,93221-01-3,93221-02-4,99630-88-3,109215-53-4,115792-70-6,115792-73-9,139894-92-1,139973-25-4,144071-49-8,147648-81-5) + Nα-(fluoren-9-ylmethoxycarbonyl)-L-serine pentafluorophenyl ester (86061-05-4) → N-(9-fluorenylmethoxycarbonyl)-3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-L-serine pentafluorophenyl ester (478062-63-4)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1021/jo026053b

Reference yield:

Nα-(fluoren-9-ylmethoxycarbonyl)-L-serine pentafluorophenyl ester (86061-05-4) + β-D-glucose pentaacetate (604-69-3) → N-(9-fluorenylmethoxycarbonyl)-3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-L-serine pentafluorophenyl ester (478062-63-4)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1016/j.tetlet.2003.10.178

upstream raw materials:

D-glucose pentaacetate

N^α-(fluoren-9-ylmethoxycarbonyl)-L-serine pentafluorophenyl ester

β-D-glucose pentaacetate

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