Carbamic acid, N-[6-[[3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-galactopyranosyl]oxy]hexyl]-, phenylmethyl ester

Base Information

• Chemical Name: Carbamic acid, N-[6-[[3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-galactopyranosyl]oxy]hexyl]-, phenylmethyl ester
• CAS No.: 159173-77-0
• Molecular Formula: C28H40N2O11
• Molecular Weight: 0
• Mol file: 159173-77-0.mol

Synonyms:Carbamic acid, N-[6-[[3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-galactopyranosyl]oxy]hexyl]-, phenylmethyl ester;N-[6-[[3,4,6-Tri-O-acetyl-2-(acetylamino)-2-deoxy-beta-D-galactopyranosyl]oxy]hexyl]carbamic acid phenylmethyl ester

Chemical Property of Carbamic acid, N-[6-[[3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-galactopyranosyl]oxy]hexyl]-, phenylmethyl ester

Chemical Property:

Purity/Quality:

99%,98%, ^*data from raw suppliers

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Technology Process of Carbamic acid, N-[6-[[3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-galactopyranosyl]oxy]hexyl]-, phenylmethyl ester

There total 18 articles about Carbamic acid, N-[6-[[3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-galactopyranosyl]oxy]hexyl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

→ 6-(N-benzyloxycarbonylamino)hexyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy)-β-D-glucopyranoside (62205-56-5,159173-77-0)

Guidance literature:

Reference yield: 83.0%

N-benzyloxycarbonyl-6-amino-1-hexanol (17996-12-2) + 2-acetamido-1,3,4,6-tetra-O-acetyl-2-deoxy-β-D-galactopyranose (3006-60-8) → 6'-(N-benzyloxycarbonyl)aminohexyl-2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-galactopyranoside (159173-77-0)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 16h;

Reference yield: 80.0%

N-benzyloxycarbonyl-6-amino-1-hexanol (17996-12-2) + Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester (3068-34-6) → 6-(N-benzyloxycarbonylamino)hexyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy)-β-D-glucopyranoside (62205-56-5,159173-77-0)

Guidance literature:

With mercury(II) cyanide; In nitromethane; benzene; for 72h; Ambient temperature;

DOI:10.1016/S0008-6215(00)85520-2

upstream raw materials:

N-benzyloxycarbonyl-6-amino-1-hexanol

Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester

Acetic acid (2R,3R,4R,5S,6R)-2,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-4-yl ester

2-methyl-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyranoso)[1,2-d]-2-oxazoline

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