5-Iodo-1,2,3-trimethylbenzene

Base Information

• Chemical Name: 5-Iodo-1,2,3-trimethylbenzene
• CAS No.: 41381-34-4
• Molecular Formula: C9H11I
• Molecular Weight: 246.091
• Mol file: 41381-34-4.mol

Synonyms:5-Iodo-1,2,3-trimethylbenzene

Chemical Property of 5-Iodo-1,2,3-trimethylbenzene

Chemical Property:

• PSA: 0.00000
• LogP: 3.21640
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

5-Iodo-1,2,3-trimethylbenzene 96% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 5-Iodo-1,2,3-trimethylbenzene

There total 1 articles about 5-Iodo-1,2,3-trimethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4,5-trimethylaniline (1639-31-2) → 5-iodo-1,2,3-trimethyl-benzene (41381-34-4)

Guidance literature:

Diazotization;

Reference yield: 72.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 5-iodo-1,2,3-trimethyl-benzene (41381-34-4) → C17H18

Guidance literature:

With 1-butyl-2,3-dimethylimidazolium tetrafluoroborate; C₁₈H₂₇Cl₂N₃OPd; triethylamine; triphenylphosphine; at 100 ℃; for 12h; regioselective reaction; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.jorganchem.2015.05.020

Reference yield:

5-iodo-1,2,3-trimethyl-benzene (41381-34-4) → 1,2,3-triiodo-4,5,6-trimethylbenzene (41694-36-4)

Guidance literature:

With sulfuric acid; iodine; periodic acid; In acetic acid;

DOI:10.1246/bcsj.46.589

upstream raw materials:

3,4,5-trimethylaniline

Downstream raw materials:

3,3',4,4',5,5'-hexamethylbiphenyl

1,2,3-triiodo-4,5,6-trimethylbenzene

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