3-Bromo-5-ethyl-2-hydroxybenzaldehyde

Base Information

Chemical Name:3-Bromo-5-ethyl-2-hydroxybenzaldehyde
CAS No.:708209-58-9
Molecular Formula:C9H9BrO2
Molecular Weight:229.073
Hs Code.:2913000090
DSSTox Substance ID:DTXSID10428276
Wikidata:Q82241090
Mol file:708209-58-9.mol

Synonyms:3-bromo-5-ethyl-2-hydroxybenzaldehyde;708209-58-9;3-Bromo-5-ethyl-2-hydroxy-benzaldehyde;BENZALDEHYDE, 3-BROMO-5-ETHYL-2-HYDROXY-;SCHEMBL5883309;DTXSID10428276;AKOS015996256;E97762

Suppliers and Price of 3-Bromo-5-ethyl-2-hydroxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

CHESS?
AD060056:3-Bromo-5-ethyl-2-hydroxy-benzaldehyde 95
5 g
$ 1020.00

Total 3 raw suppliers

Chemical Property of 3-Bromo-5-ethyl-2-hydroxybenzaldehyde

Chemical Property:

PSA：37.30000
LogP:2.52960
XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:227.97859
Heavy Atom Count:12
Complexity:161

Purity/Quality:

99% ^*data from raw suppliers

AD060056:3-Bromo-5-ethyl-2-hydroxy-benzaldehyde 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1=CC(=C(C(=C1)Br)O)C=O

Technology Process of 3-Bromo-5-ethyl-2-hydroxybenzaldehyde

There total 2 articles about 3-Bromo-5-ethyl-2-hydroxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 52411-35-5
5-ethyl-2-hydroxybenzaldehyde

: 708209-58-9
3-bromo-5-ethylsalicylaldehyde

Guidance literature:: With bromine; sodium acetate; acetic acid; at 50 ℃; for 12h;
DOI:10.1016/j.tetasy.2004.03.010

Reference yield:

: 123-07-9
4-Ethylphenol

: 708209-58-9
3-bromo-5-ethylsalicylaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg(OMe)2 / methanol

1.2: methanol; toluene / 2 h / 95 - 105 °C

1.3: 80 percent / aq. H₂SO₄ / methanol; toluene / 2 h / 50 °C

2.1: 88 percent / glacial acetic acid; NaOAc; Br₂ / 12 h / 50 °C

With bromine; sodium acetate; magnesium methanolate; acetic acid; In methanol;
DOI:10.1016/j.tetasy.2004.03.010