2(3H)-Furanone,3-aminodihydro-3,5-dimethyl-,(3S-trans)-(9CI)

Base Information

• Chemical Name: 2(3H)-Furanone,3-aminodihydro-3,5-dimethyl-,(3S-trans)-(9CI)
• CAS No.: 160281-12-9
• Molecular Formula: C₆H₁₁NO₂
• Molecular Weight: 129.159
• Mol file: 160281-12-9.mol

Synonyms:2(3H)-Furanone,3-aminodihydro-3,5-dimethyl-,(3S-trans)-(9CI)

Chemical Property of 2(3H)-Furanone,3-aminodihydro-3,5-dimethyl-,(3S-trans)-(9CI)

Chemical Property:

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Technology Process of 2(3H)-Furanone,3-aminodihydro-3,5-dimethyl-,(3S-trans)-(9CI)

There total 4 articles about 2(3H)-Furanone,3-aminodihydro-3,5-dimethyl-,(3S-trans)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.6%

N-Benzoyl-(S)-α-(2-propenyl)-α-alanine (160281-26-5) → (S)-α-allylalanine (96886-55-4) + (2S,4S)-2-Amino-2,4-dimethylbutyrolactone (160281-12-9,160281-13-0) + (2S,4R)-2-Amino-2,4-dimethylbutyrolactone (160281-12-9,160281-13-0)

Guidance literature:

With hydrogenchloride; at 145 ℃; for 2h;

DOI:10.1021/jo00094a038

Reference yield: 61.6%

N-Benzoyl-(S)-α-(2-propenyl)-α-alanine (160281-26-5) → (S)-α-allylalanine (96886-55-4) + (2S,4S)-2-Amino-2,4-dimethylbutyrolactone (160281-12-9,160281-13-0) + (2S,4R)-2-Amino-2,4-dimethylbutyrolactone (160281-12-9,160281-13-0)

Guidance literature:

With hydrogenchloride; at 145 ℃; for 2h;

DOI:10.1021/jo00094a038

Reference yield:

2-Amino-2-methyl-pent-4-enoic acid ethyl ester (114968-87-5,165035-97-2) → (S)-α-allylalanine (96886-55-4) + (R)-α-(2-Propenyl)-α-alanine ethyl ester (165035-97-2) + (2S,4S)-2-Amino-2,4-dimethylbutyrolactone (160281-12-9,160281-13-0) + (2S,4R)-2-Amino-2,4-dimethylbutyrolactone (160281-12-9,160281-13-0)

Guidance literature:

With sodium hydroxide; at 37 ℃; for 20h; α-chymotrypsin, pH 7.5-8;

DOI:10.1021/jo00094a038

upstream raw materials:

2-Amino-2-methyl-pent-4-enoic acid ethyl ester

N-Benzoyl-(S)-α-(2-propenyl)-α-alanine

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