3-Chlorophenyl 4-chlorophenylamine

Base Information

Chemical Name:3-Chlorophenyl 4-chlorophenylamine
CAS No.:15979-79-0
Molecular Formula:C12H9 Cl2 N
Molecular Weight:238.116
Hs Code.:2921420090
Mol file:15979-79-0.mol

Synonyms:Diphenylamine,3,4'-dichloro- (8CI); 3,4'-Dichlorodiphenylamine

Suppliers and Price of 3-Chlorophenyl 4-chlorophenylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-Chlorophenyl 4-chlorophenylamine

Chemical Property:

Vapor Pressure:6.4E-05mmHg at 25°C
Boiling Point:344.9°Cat760mmHg
Flash Point:162.4°C
PSA：12.03000
Density:1.327g/cm³
LogP:4.81000

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Chlorophenyl 4-chlorophenylamine

There total 3 articles about 3-Chlorophenyl 4-chlorophenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 108-37-2
1-bromo-3-chlorobenzene

: 106-47-8
4-chloro-aniline

: 15979-79-0
3-chloro-N-(4-chlorophenyl)aniline

Guidance literature:: With potassium phosphate; methanesulfonato(2-dicyclohexylphosphino-3,6-dimethoxy-2',4',6'-tri-i-propyl-1,1'-biphenyl)(2'-methylamino-1,1'-biphenyl-2-yl)palladium(II); In 1,4-dioxane; water; at 150 ℃; for 0.25h; under 10343.2 Torr; Flow reactor;
DOI:10.1021/acs.orglett.9b02259

Reference yield:

: N-(3-chloro-phenyl)-benzimidic acid-(4-chloro-phenyl ester)

: 15979-79-0
3-chloro-N-(4-chlorophenyl)aniline

Guidance literature:: at 290 ℃; und Erwaermen des erhaltenen N-<3-Chlor-phenyl>-N-<4-chlor-phenyl>-benzamids mit wss.-aethanol. Kalilauge;
DOI:10.1039/jr9310000294

Reference yield:

: 34918-77-9
N-(3-chlorophenyl)benzimidoyl chloride

: 15979-79-0
3-chloro-N-(4-chlorophenyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether; ethanol

2: 290 °C / und Erwaermen des erhaltenen N-<3-Chlor-phenyl>-N-<4-chlor-phenyl>-benzamids mit wss.-aethanol. Kalilauge

With diethyl ether; ethanol;
DOI:10.1039/jr9310000294