N-[[(Benzyl)oxy]carbonyl]-3-[(2-O,3-O,4-O,6-O-tetraacetyl-β-D-galactopyranosyl)oxy]-L-alanine methyl ester

Base Information

Chemical Name:N-[[(Benzyl)oxy]carbonyl]-3-[(2-O,3-O,4-O,6-O-tetraacetyl-β-D-galactopyranosyl)oxy]-L-alanine methyl ester
CAS No.:14364-68-2
Molecular Formula:C₂₆H₃₃NO₁₄
Molecular Weight:583.53852
Hs Code.:
Mol file:14364-68-2.mol

Synonyms:N-[[(Benzyl)oxy]carbonyl]-3-[(2-O,3-O,4-O,6-O-tetraacetyl-β-D-galactopyranosyl)oxy]-L-alanine methyl ester

Suppliers and Price of N-[[(Benzyl)oxy]carbonyl]-3-[(2-O,3-O,4-O,6-O-tetraacetyl-β-D-galactopyranosyl)oxy]-L-alanine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[[(Benzyl)oxy]carbonyl]-3-[(2-O,3-O,4-O,6-O-tetraacetyl-β-D-galactopyranosyl)oxy]-L-alanine methyl ester

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Technology Process of N-[[(Benzyl)oxy]carbonyl]-3-[(2-O,3-O,4-O,6-O-tetraacetyl-β-D-galactopyranosyl)oxy]-L-alanine methyl ester

There total 2 articles about N-[[(Benzyl)oxy]carbonyl]-3-[(2-O,3-O,4-O,6-O-tetraacetyl-β-D-galactopyranosyl)oxy]-L-alanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1676-81-9
N-benzyloxycarbonyl-L-serine methyl ester

: 55692-87-0
isopropyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-galactopyranoside

: 14364-68-2
O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-N-benzyloxycarbonyl-L-serine methyl ester

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1039/b108399f

Reference yield:

: 367-93-1
isopropyl β-D-thiogalactopyranoside

: 14364-68-2
O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-N-benzyloxycarbonyl-L-serine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / pyridine

2: 87 percent / NIS; TMSOTf / CH₂Cl₂ / 2 h / 0 °C

With pyridine; N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane;
DOI:10.1039/b108399f