(S)-1-(2-Methoxyphenyl)ethanamine hydrochloride

Base Information

• Chemical Name: (S)-1-(2-Methoxyphenyl)ethanamine hydrochloride
• CAS No.: 1332832-15-1
• Molecular Formula: C₉H₁₃NO*ClH
• Molecular Weight: 187.669
• Mol file: 1332832-15-1.mol

Synonyms:(S)-1-(2-METHOXYPHENYL)ETHANAMINE HYDROCHLRIDE;(1S)-1-(2-methoxyphenyl)ethanamine,hydrochloride;Benzenemethanamine, 2-methoxy-α-methyl-, hydrochloride (1:1), (αS)-

Chemical Property of (S)-1-(2-Methoxyphenyl)ethanamine hydrochloride

Chemical Property:

• PSA: 35.25000
• LogP: 3.21720
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

(S)-1-(2-Methoxyphenyl)EthanamineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (S)-1-(2-Methoxyphenyl)ethanamine hydrochloride

There total 3 articles about (S)-1-(2-Methoxyphenyl)ethanamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+/-)-2-methoxy-α-methylbenzylamine hydrochloride (17087-50-2,704892-60-4) → (S)-1-(2-methoxyphenyl)ethanamine hydrochloride (1332832-15-1,704892-60-4) + (-)-[(1R)-1-(2-methoxyphenyl)ethyl]amine hydrochloride (704892-60-4)

Guidance literature:

With chiral stationary phase including isopropyl-functionalized CF₆; In methanol; acetic acid; triethylamine; acetonitrile; at 20 ℃; Purification / work up;

Reference yield:

C9H11NO*ClH (1164111-48-1) → (S)-1-(2-methoxyphenyl)ethanamine hydrochloride (1332832-15-1,704892-60-4) + (-)-[(1R)-1-(2-methoxyphenyl)ethyl]amine hydrochloride (704892-60-4)

Guidance literature:

With chloro(1,5-cyclooctadiene)rhodium(I) dimer; zhaophos; hydrogen; In isopropyl alcohol; at 25 ℃; for 24h; under 7600.51 Torr; Overall yield = 82%; enantioselective reaction; Inert atmosphere; Glovebox; Autoclave;

DOI:10.1002/anie.201404570

Reference yield:

(S)-1-(2-methoxyphenyl)ethanamine (40023-74-3,62409-14-7,68285-23-4,68285-24-5) → (S)-1-(2-methoxyphenyl)ethanamine hydrochloride (1332832-15-1,704892-60-4)

Guidance literature:

With hydrogenchloride; In dichloromethane; water;

DOI:10.1002/adsc.201100250

upstream raw materials:

(+/-)-2-methoxy-α-methylbenzylamine hydrochloride

(S)-1-(2-methoxyphenyl)ethanamine

C₉H₁₁NO*ClH

Downstream raw materials:

(S)-2,2,2-trifluoro-N-(1-(2-methoxyphenyl)ethyl)acetamide

(S)-[1-(2-methoxy-phenyl)-ethyl]pyridin-2-ylmethylamine

(S)-1-(2-methoxyphenyl)ethanamine

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