ETHYL 1-ETHYL-4-OXO-3-PIPERIDINECARBOXYLATE HYDROCHLORIDE

Base Information

• Chemical Name: ETHYL 1-ETHYL-4-OXO-3-PIPERIDINECARBOXYLATE HYDROCHLORIDE
• CAS No.: 99329-51-8
• Molecular Formula: C10H18ClNO3
• Molecular Weight: 199.25
• Hs Code.: 2933399090
• Mol file: 99329-51-8.mol

Synonyms:ETHYL 1-ETHYL-4-OXO-3-PIPERIDINECARBOXYLATE HYDROCHLORIDE;ethyl 1-ethyl-4-oxo-3-piperidinecarboxylate hydrochloride(SALTDATA: HCl);1-ethyl-4-oxo-3-Piperidinecarboxylic acid ethyl ester

Chemical Property of ETHYL 1-ETHYL-4-OXO-3-PIPERIDINECARBOXYLATE HYDROCHLORIDE

Chemical Property:

• Vapor Pressure: 0.00223mmHg at 25°C
• Boiling Point: 289.2°C at 760 mmHg
• Flash Point: 128.7°C
• PSA: 46.61000
• Density: 1.072g/cm³
• LogP: 1.20030

Purity/Quality:

98% ^*data from raw suppliers

Ethyl1-ethyl-4-oxopiperidine-3-carboxylatehydrochloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ETHYL 1-ETHYL-4-OXO-3-PIPERIDINECARBOXYLATE HYDROCHLORIDE

There total 3 articles about ETHYL 1-ETHYL-4-OXO-3-PIPERIDINECARBOXYLATE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

ethyl 3-[N-ethyl-N-(2-ethoxycarbonylethyl)amino]propionate (3619-64-5) → ethyl 1-ethyl-4-oxopiperidine-3-carboxylate (99329-51-8)

Guidance literature:

With sodium hydride; In ethanol; toluene; Heating;

DOI:10.1016/S0960-894X(02)00228-7

Reference yield:

Ethyl 3-bromopropionate (539-74-2) → ethyl 1-ethyl-4-oxopiperidine-3-carboxylate (99329-51-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 84 percent / Et₃N / acetonitrile / 80 °C

2: 100 percent / NaH / toluene; ethanol / Heating

With sodium hydride; triethylamine; In ethanol; toluene; acetonitrile; 2: Dieckmann reaction;

DOI:10.1016/S0960-894X(02)00228-7

Reference yield:

→ ethyl 1-ethyl-4-oxopiperidine-3-carboxylate (99329-51-8)

Guidance literature:

/BRN= 144582/;

upstream raw materials:

ethyl 3-[N-ethyl-N-(2-ethoxycarbonylethyl)amino]propionate

Ethyl 3-bromopropionate

Downstream raw materials:

N-ethyl-4-piperidone

(2-amino-6-ethyl-4,5,6,7-tetrahydro-thieno[2,3-c]pyridin-3-yl)-(2-chloro-phenyl)-methanone

N-[3-(2-chloro-benzoyl)-6-ethyl-4,5,6,7-tetrahydro-thieno[2,3-c]pyridin-2-yl]-isobutyramide

4-amino-N-ethylpiperidine

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