9-Methyl-1-undecene

Base Information

Chemical Name:9-Methyl-1-undecene
CAS No.:74630-41-4
Molecular Formula:C₁₂H₂₄
Molecular Weight:168.323
Hs Code.:
Mol file:74630-41-4.mol

Synonyms:9-Methyl-1-undecene

Suppliers and Price of 9-Methyl-1-undecene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 9-Methyl-1-undecene

Chemical Property:

Melting Point:-38.4°C (estimate)
Refractive Index:1.4260 (estimate)
Boiling Point:207.3°C (estimate)
PSA：0.00000
Density:0.7761 (estimate)
LogP:4.55910

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 9-Methyl-1-undecene

There total 3 articles about 9-Methyl-1-undecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 78-76-2,5787-31-5
s-butyl bromide

: 889882-46-6
oct-7-en-1-yl 4-methylbenzenesulfonate

: 74630-41-4
9-methylundec-1-ene

Guidance literature:: s-butyl bromide; With iodine; magnesium; In tetrahydrofuran; at 25 ℃; for 1h;

oct-7-en-1-yl 4-methylbenzenesulfonate; With dilithium tetrachlorocuprate; In tetrahydrofuran; at -78 - 25 ℃; for 14h; Inert atmosphere;
DOI:10.1002/anie.201611940

Reference yield: 79.0%

: 1647-16-1
1,10-decadiene

: 97-93-8
triethylaluminum

: 107771-00-6
3,10-dimethylundecane

: 74630-41-4
9-methylundec-1-ene

Guidance literature:: 1,10-decadiene; triethylaluminum; With zirconocene dichloride; In toluene; at 40 ℃; for 4h;

With water; Acidic conditions;
DOI:10.1007/s11172-015-1182-1

Reference yield:

: 13175-44-5
oct-7-en-1-ol

: 74630-41-4
9-methylundec-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / chloroform; dichloromethane / 14 h / 25 °C

2.1: magnesium; iodine / tetrahydrofuran / 1 h / 25 °C

2.2: 14 h / -78 - 25 °C / Inert atmosphere

With pyridine; iodine; magnesium; In tetrahydrofuran; dichloromethane; chloroform;
DOI:10.1002/anie.201611940