methyl 4-(acetyloxy)-8-bromo-5-(propan-2-yloxy)naphthalene-2-carboxylate

Base Information

Chemical Name:methyl 4-(acetyloxy)-8-bromo-5-(propan-2-yloxy)naphthalene-2-carboxylate
CAS No.:225114-49-8
Molecular Formula:C₁₇H₁₇BrO₅
Molecular Weight:381.223
Hs Code.:

Synonyms:2-Naphthalenecarboxylic acid, 4-(acetyloxy)-8-broMo-5-(1-Methylethoxy)-, Methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-(acetyloxy)-8-bromo-5-(propan-2-yloxy)naphthalene-2-carboxylate

Chemical Property:

Vapor Pressure:1.2E-09mmHg at 25°C
Boiling Point:487.3°C at 760 mmHg
Flash Point:248.5°C
PSA：61.83000
Density:1.398g/cm³
LogP:4.10140

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl 4-(acetyloxy)-8-bromo-5-(propan-2-yloxy)naphthalene-2-carboxylate

There total 1 articles about methyl 4-(acetyloxy)-8-bromo-5-(propan-2-yloxy)naphthalene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 108-24-7
acetic anhydride

: 2-[1-(2-Bromo-5-isopropoxy-phenyl)-meth-(E)-ylidene]-succinic acid 1-methyl ester

: 225114-49-8
Methyl 4-acetoxy-8-bromo-5-isopropoxy-2-naphthoate

Guidance literature:: With sodium acetate; for 6h; Heating;
DOI:10.1039/a908367g

Reference yield: 95.0%

: 225114-49-8
Methyl 4-acetoxy-8-bromo-5-isopropoxy-2-naphthoate

: 267881-57-2
8-bromo-4-hydroxy-5-isopropoxy-naphthalene-2-carboxylic acid methyl ester

Guidance literature:: With potassium hydroxide; In methanol; for 1h;
DOI:10.1039/a908367g

Reference yield:

: 225114-49-8
Methyl 4-acetoxy-8-bromo-5-isopropoxy-2-naphthoate

: 267881-58-3
Methyl 8-bromo-5-isopropoxy-4-methoxy-2-naphthoate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / KOH / methanol / 1 h

2: 99 percent / t-BuOK / acetone / 18 h / Heating

With potassium hydroxide; potassium tert-butylate; In methanol; acetone; 1: Deacylation / 2: Etherification;
DOI:10.1039/a908367g