2-aminobenzo[d]oxazol-5-ylboronic acid hydrochloride

Base Information

• Chemical Name: 2-aminobenzo[d]oxazol-5-ylboronic acid hydrochloride
• CAS No.: 1224844-65-8
• Molecular Formula: C7H8BClN2O3
• Molecular Weight: 177.955
• Hs Code.: 2934999090
• Mol file: 1224844-65-8.mol

Synonyms:2-aminobenzo[d]oxazol-5-ylboronic acid hydrochloride;2-aminobenzo[d]oxazol-5-ylboronic acid hydrochlorid

Chemical Property of 2-aminobenzo[d]oxazol-5-ylboronic acid hydrochloride

Chemical Property:

• PSA: 93.24000
• LogP: -0.17810
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

99%, ^*data from raw suppliers

2-Aminobenzo[d]oxazol-5-ylboronicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-aminobenzo[d]oxazol-5-ylboronic acid hydrochloride

There total 3 articles about 2-aminobenzo[d]oxazol-5-ylboronic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.4%

tetrahydroxydiboron (13675-18-8) + 5-bromo-1,3-benzoxazol-2-amine (64037-07-6) → 2-aminobenzo[d]oxazol-5-ylboronic acid (1224844-65-8)

Guidance literature:

With chloro[(tri-tert-butylphosphine)-2-(2-aminobiphenyl)]palladium (II); potassium acetate; In methanol; water; ethylene glycol; at 35 ℃; Solvent; Temperature; Inert atmosphere; Large scale;

DOI:10.1021/acs.oprd.6b00345

Reference yield:

tetrahydroxydiboron (13675-18-8) + 5-bromo-1,3-benzoxazol-2-amine (64037-07-6) → 1,3-benzoxazol-2-amine (4570-41-6) + 2-aminobenzo[d]oxazol-5-ylboronic acid (1224844-65-8)

Guidance literature:

With chloro[(tri-tert-butylphosphine)-2-(2-aminobiphenyl)]palladium (II); potassium acetate; In methanol; water; ethylene glycol; at 65 ℃; for 4h; Inert atmosphere;

DOI:10.1021/acs.oprd.6b00345

Reference yield:

tetrahydroxydiboron (13675-18-8) + 5-bromo-1,3-benzoxazol-2-amine (64037-07-6) → 1,3-benzoxazol-2-amine (4570-41-6) + 2-aminobenzo[d]oxazol-5-ylboronic acid (1224844-65-8) + C14H10N4O2

Guidance literature:

With chloro[(tri-tert-butylphosphine)-2-(2-aminobiphenyl)]palladium (II); potassium acetate; In methanol; water; ethylene glycol; at 65 ℃; for 16h; Inert atmosphere;

DOI:10.1021/acs.oprd.6b00345

upstream raw materials:

tetrahydroxydiboron

5-bromo-1,3-benzoxazol-2-amine

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