Imidodisulfuric acid, phenyl-

Base Information

• Chemical Name: Imidodisulfuric acid, phenyl-
• CAS No.: 21250-88-4
• Molecular Formula: C6H7NO6S2
• Molecular Weight: 253.25
• Mol file: 21250-88-4.mol

Synonyms:Imidodisulfuric acid, phenyl-

Chemical Property of Imidodisulfuric acid, phenyl-

Chemical Property:

• PSA: 128.74000
• LogP: 2.26020

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Imidodisulfuric acid, phenyl-

There total 2 articles about Imidodisulfuric acid, phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

aniline (62-53-3) → Tf2N-phenyl (21250-88-4)

Guidance literature:

With sulfur trioxide; triethylamine;

DOI:10.1246/bcsj.47.2713

Reference yield:

→ Tf2N-phenyl (21250-88-4)

Guidance literature:

Anilin, SO3, α-Picolin; (im Gemisch m. Anilin-N-sulfonsaeure);

Reference yield:

3,3-ethylenedioxy-5α-hydroxy-11β-(4-hydroxy-phenyl)-estr-9-en-17-one + Tf2N-phenyl (21250-88-4) → 3,3-ethylenedioxy-5α-hydroxy-11β-(4-hydroxy-phenyl)-estr-9-en-17-one

Guidance literature:

3,3-ethylenedioxy-5α-hydroxy-11β-(4-hydroxy-phenyl)-estr-9-en-17-one; With sodium hydride; In tetrahydrofuran; at -78 ℃; for 0.166667h;

Tf₂N-phenyl; In tetrahydrofuran; at 20 ℃; for 16h;

upstream raw materials:

aniline