2-(4-broMobenzyl)propanoic acid

Base Information

• Chemical Name: 2-(4-broMobenzyl)propanoic acid
• CAS No.: 66735-01-1
• Molecular Formula: C10H11BrO2
• Molecular Weight: 243
• Hs Code.: 2916399090

Synonyms:2-(4-broMobenzyl)propanoic acid;3-(4-Bromophenyl)-2-methylpropanoic acid;3-(4-Bromophenyl)-2-methylpropionic acid, 2-(4-Bromobenzyl)propanoic acid

Chemical Property of 2-(4-broMobenzyl)propanoic acid

Chemical Property:

• PSA: 37.30000
• LogP: 2.71230
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

2-(4-Bromobenzyl)propanoicacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(4-broMobenzyl)propanoic acid

There total 4 articles about 2-(4-broMobenzyl)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(4-bromobenzyl)-2-methylmalonic acid diethyl ester (70146-85-9) → 3-(4-bromophenyl)-2-methylpropanoic acid (66735-01-1)

Guidance literature:

In sodium hydroxide; ethanol; water;

Reference yield:

propionic acid (802294-64-0,79-09-4) + 1-bromomethyl-4-bromobenzene (589-15-1) → 3-(4-bromophenyl)-2-methylpropanoic acid (66735-01-1)

Guidance literature:

propionic acid; With lithium diisopropyl amide; In tetrahydrofuran; at 0 - 80 ℃; for 2h; Inert atmosphere;

1-bromomethyl-4-bromobenzene; In tetrahydrofuran; at 0 - 80 ℃; Inert atmosphere;

DOI:10.1021/acs.orglett.0c03794

Reference yield:

4-Brom-α-methyl-zimtsaeure (66735-14-6) → 3-(4-bromophenyl)-2-methylpropanoic acid (66735-01-1)

Guidance literature:

With hydrogen;

DOI:10.1021/jacs.9b13876

upstream raw materials:

2-(4-bromobenzyl)-2-methylmalonic acid diethyl ester

4-Brom-α-methyl-zimtsaeure

propionic acid

1-bromomethyl-4-bromobenzene

Downstream raw materials:

2-methyl-3-(4-bromophenyl)propanol

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