CHEMBRDG-BB 4015415

Base Information

• Chemical Name: CHEMBRDG-BB 4015415
• CAS No.: 22359-13-3
• Molecular Formula: C7H9ClN2O2
• Molecular Weight: 188.614
• Hs Code.: 2933599090
• Mol file: 22359-13-3.mol

Synonyms:CHEMBRDG-BB 4015415;3-(2-CHLOROETHYL)-6-METHYLPYRIMIDINE-2,4(1H,3H)-DIONE;3-(2-chloroethyl)-6-methylpyrimidine-2,4(1H,3H)-dione(SALTDATA: FREE)

Chemical Property of CHEMBRDG-BB 4015415

Chemical Property:

• PSA: 54.86000
• Density: 1.284g/cm³
• LogP: 0.08380

Purity/Quality:

99% ^*data from raw suppliers

3-(2-chloroethyl)-6-methylpyrimidine-2,4(1H,3H)-dione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CHEMBRDG-BB 4015415

There total 3 articles about CHEMBRDG-BB 4015415 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3,4-dihydro-6-methyl-2-methylthio-4-oxo-3-pyrimidinyl)(6-methyl-2-methylthiopyrimidinyloxy)ethane → 6-Methyluracil (626-48-2) + 6-methyl-3-(β-chloroethyl)uracil (22359-13-3) + 6-methyl-3-(β-hydroxyethyl)uracil (20551-25-1)

Guidance literature:

With hydrogenchloride; Heating;

DOI:10.1007/BF00702146

Reference yield:

4-Hydroxy-6-methyl-2-methylthiopyrimidine (6328-58-1) → 6-methyl-3-(β-chloroethyl)uracil (22359-13-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 82 percent / Na / butan-1-ol; dimethylformamide / 30 - 35 °C

2: aq. HCl / Heating

With hydrogenchloride; sodium; In N,N-dimethyl-formamide; butan-1-ol;

DOI:10.1007/BF00702146

Reference yield:

→ 6-methyl-3-(β-chloroethyl)uracil (22359-13-3)

Guidance literature:

3-<2-Hydroxy-ethyl>-6-methyl-uracil, SOCl2;

upstream raw materials:

4-Hydroxy-6-methyl-2-methylthiopyrimidine

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