Pyrene-13C16

Base Information

Chemical Name:Pyrene-13C16
CAS No.:1228182-40-8
Molecular Formula:C16H10
Molecular Weight:218.3946
Hs Code.:

Synonyms:Pyrene-13C16

Suppliers and Price of Pyrene-13C16

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
PYRENE-13C16 95.00%
5MG
$ 496.71

Total 1 raw suppliers

Chemical Property of Pyrene-13C16

Chemical Property:

PSA：0.00000
LogP:4.58400

Purity/Quality:

98% by CP; 99% atom 13C ^*data from raw suppliers

PYRENE-13C16 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses Pyrene-13C16 is the labeled analogue of Pyrene (P849000). Pyrene occurs in coal tar. Also obtained by the destructive hydrogenation of hard coal. Found in wastewater in aquatic environments, and possesses genotoxic characteristics relating to estrogenic/androgenic, antiestrogenic and antiandrogenic activity. Pyrene-13C16 is a contaminant of emerging concern (CECs).

Technology Process of Pyrene-13C16

There total 13 articles about Pyrene-13C16 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ⁽¹³⁾C₁₆H₁₂O

: 1228182-40-8,1173023-76-1
U-(13)C-pyrene

Guidance literature:: With methanesulfonic acid; In dichloromethane; at 20 ℃; for 0.5h; Cooling with ice;
DOI:10.1039/c0ob01107j

Reference yield:

: 32488-44-1
benzene-⁽¹³⁾C₆

: 1228182-40-8,1173023-76-1
U-(13)C-pyrene

Guidance literature:: Multi-step reaction with 13 steps

1.1: aluminum (III) chloride / 1,1,2,2-tetrachloroethane

2.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C

2.2: 120 - 215 °C

3.1: methanesulfonic acid / 0.5 h / 90 °C / Inert atmosphere

4.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C

4.2: 120 - 215 °C

5.1: aluminum (III) chloride / 1,1,2,2-tetrachloroethane / 20 °C / Cooling with ice

6.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C

6.2: 120 - 215 °C

7.1: sulfuric acid / Reflux

8.1: palladium 10% on activated carbon / Triethylene glycol dimethyl ether / 4 h / 240 °C / Inert atmosphere

9.1: methanesulfonic acid / 0.5 h / 90 °C / Inert atmosphere

10.1: n-butyllithium; N-cyclohexylisopropylamine / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

10.2: 1 h / -78 °C / Inert atmosphere

11.1: palladium 10% on activated carbon / Triethylene glycol dimethyl ether / 4 h / 240 °C / Inert atmosphere

12.1: diisobutylaluminium hydride / hexane; toluene / 1 h / -78 °C / Inert atmosphere

12.2: Inert atmosphere

13.1: methanesulfonic acid / dichloromethane / 0.5 h / 20 °C / Cooling with ice

With aluminum (III) chloride; n-butyllithium; methanesulfonic acid; sulfuric acid; N-cyclohexylisopropylamine; palladium 10% on activated carbon; diisobutylaluminium hydride; hydrazine hydrate; In tetrahydrofuran; Triethylene glycol dimethyl ether; hexane; dichloromethane; toluene; 1,1,2,2-tetrachloroethane; diethylene glycol; 2.1: Wolff-Kishner reduction / 2.2: Wolff-Kishner reduction / 4.1: Wolff-Kishner reduction / 4.2: Wolff-Kishner reduction / 5.1: Friedel-Crafts acylation / 6.1: Wolff-Kishner reduction / 6.2: Wolff-Kishner reduction;
DOI:10.1039/c0ob01107j

Reference yield:

: 1323432-98-9
U-⁽¹³⁾C-4-oxo-4-(5,6,7,8-tetrahydronaphthalen-2-yl)butanoic acid

: 1228182-40-8,1173023-76-1
U-(13)C-pyrene

Guidance literature:: Multi-step reaction with 8 steps

1.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C

1.2: 120 - 215 °C

2.1: sulfuric acid / Reflux

3.1: palladium 10% on activated carbon / Triethylene glycol dimethyl ether / 4 h / 240 °C / Inert atmosphere

4.1: methanesulfonic acid / 0.5 h / 90 °C / Inert atmosphere

5.1: n-butyllithium; N-cyclohexylisopropylamine / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

5.2: 1 h / -78 °C / Inert atmosphere

6.1: palladium 10% on activated carbon / Triethylene glycol dimethyl ether / 4 h / 240 °C / Inert atmosphere

7.1: diisobutylaluminium hydride / hexane; toluene / 1 h / -78 °C / Inert atmosphere

7.2: Inert atmosphere

8.1: methanesulfonic acid / dichloromethane / 0.5 h / 20 °C / Cooling with ice

With n-butyllithium; methanesulfonic acid; sulfuric acid; N-cyclohexylisopropylamine; palladium 10% on activated carbon; diisobutylaluminium hydride; hydrazine hydrate; In tetrahydrofuran; Triethylene glycol dimethyl ether; hexane; dichloromethane; toluene; diethylene glycol; 1.1: Wolff-Kishner reduction / 1.2: Wolff-Kishner reduction;
DOI:10.1039/c0ob01107j