7-BROMO-2-(BROMOMETHYL)BENZOTHIAZOLE

Base Information

• Chemical Name: 7-BROMO-2-(BROMOMETHYL)BENZOTHIAZOLE
• CAS No.: 110704-15-9
• Molecular Formula: C₈H₅Br₂NS
• Molecular Weight: 307.008
• Mol file: 110704-15-9.mol

Synonyms:7-BROMO-2-(BROMOMETHYL)BENZOTHIAZOLE;7-BroMo-2-(broMoMethyl)benzo[d]thiazole

Chemical Property of 7-BROMO-2-(BROMOMETHYL)BENZOTHIAZOLE

Chemical Property:

• PSA: 41.13000
• LogP: 3.95370

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7-BROMO-2-(BROMOMETHYL)BENZOTHIAZOLE

There total 2 articles about 7-BROMO-2-(BROMOMETHYL)BENZOTHIAZOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7-bromo-2-methylbenzothiazole (110704-32-0) → 7-Bromo-2-bromomethyl-benzothiazole (110704-15-9)

Guidance literature:

With N-Bromosuccinimide; Perbenzoic acid; In tetrachloromethane; for 14h; Heating; Irradiation;

DOI:10.1021/jm00105a018

Reference yield:

3-bromothioacetanilide (29452-12-8) → 7-Bromo-2-bromomethyl-benzothiazole (110704-15-9)

Guidance literature:

Multi-step reaction with 2 steps

1: K₃Fe(CN)6

2: NBS, benzoyl peroxide / CCl₄ / 14 h / Heating; Irradiation

With N-Bromosuccinimide; Perbenzoic acid; potassium hexacyanoferrate(III); In tetrachloromethane;

DOI:10.1021/jm00105a018

upstream raw materials:

7-bromo-2-methylbenzothiazole

3-bromothioacetanilide

Refernces