Cyclohexanecarboxamide, 4-amino-3-fluoro-, (1R,3S,4R)- (9CI)

Base Information

• Chemical Name: Cyclohexanecarboxamide, 4-amino-3-fluoro-, (1R,3S,4R)- (9CI)
• CAS No.: 643069-85-6
• Molecular Formula: C7H13FN2O
• Molecular Weight: 160.191
• Mol file: 643069-85-6.mol

Synonyms:Cyclohexanecarboxamide, 4-amino-3-fluoro-, (1R,3S,4R)- (9CI)

Chemical Property of Cyclohexanecarboxamide, 4-amino-3-fluoro-, (1R,3S,4R)- (9CI)

Chemical Property:

• PSA: 69.11000
• LogP: 1.33780

Purity/Quality:

99%+ ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexanecarboxamide, 4-amino-3-fluoro-, (1R,3S,4R)- (9CI)

There total 1 articles about Cyclohexanecarboxamide, 4-amino-3-fluoro-, (1R,3S,4R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1R,3S,4R)-3-fluoro-4-((R)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide (643069-83-4) → (1R,3S,4R)-4-amino-3-fluoro-cyclohexanecarboxylic acid amide (643069-85-6)

Guidance literature:

With hydrogen; palladium(II) hydroxide/carbon; In ethanol; for 16h; under 2585.81 Torr;

Reference yield:

(1R,3S,4R)-4-amino-3-fluoro-cyclohexanecarboxylic acid amide (643069-85-6) + di-tert-butyl dicarbonate (24424-99-5) → ((1R,2S,4R)-4-carbamoyl-2-fluoro-cyclohexyl)-carbamic acid tert-butyl ester (643069-87-8)

Guidance literature:

In dichloromethane; for 4h;

upstream raw materials:

(1R,3S,4R)-3-fluoro-4-((R)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide

Downstream raw materials:

((1R,2S,4R)-4-carbamoyl-2-fluoro-cyclohexyl)-carbamic acid tert-butyl ester

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