3β-Acetylamino-5α-cholestane

Base Information

• Chemical Name: 3β-Acetylamino-5α-cholestane
• CAS No.: 1912-64-7
• Molecular Formula: C₂₉H₅₁NO
• Molecular Weight: 429.73
• Mol file: 1912-64-7.mol

Synonyms:3β-Acetylamino-5α-cholestane

Chemical Property of 3β-Acetylamino-5α-cholestane

Chemical Property:

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3β-Acetylamino-5α-cholestane

There total 29 articles about 3β-Acetylamino-5α-cholestane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3β-amino-5α-cholestane (2206-21-5) → 3β-(acetylamino)-5α-cholestane (1912-64-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 250 mg / various solvent(s) / 2 h

2: 5 mg / 19 h / Heating

In various solvent(s);

DOI:10.1021/jo00337a055

Reference yield:

3α-aminocholestane → 3β-(acetylamino)-5α-cholestane (1912-64-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 400 mg / pyridine / 2 h / Heating

2: 70 mg / 10percent NaOH / aq. ethanol / 1 h / Heating

With pyridine; sodium hydroxide; In ethanol;

DOI:10.1021/jo00337a055

Reference yield:

3β-(Diacetylamido)cholestane (79483-40-2) → 3β-(acetylamino)-5α-cholestane (1912-64-7)

Guidance literature:

With sodium hydroxide; In ethanol; for 1h; Heating;

DOI:10.1021/jo00337a055

upstream raw materials:

ammonium acetate

cholestan-3-one

N-acetyl-cholest-5-en-3β-amine

N-cholest-4-en-3β-yl-acetamide

Downstream raw materials:

5α-cholestan-3β-yldimethylamine