Tributyl(2-methoxyethyl)phosphonium Bis(trifluoromethanesulfonyl)imide

Base Information

• Chemical Name: Tributyl(2-methoxyethyl)phosphonium Bis(trifluoromethanesulfonyl)imide
• CAS No.: 959698-44-3
• Molecular Formula: C₂F₆NO₄S₂*C₁₅H₃₄OP
• Molecular Weight: 541.557
• Mol file: 959698-44-3.mol

Synonyms:Tributyl(2-methoxyethyl)phosphonium Bis(trifluoromethanesulfonyl)imide

Chemical Property of Tributyl(2-methoxyethyl)phosphonium Bis(trifluoromethanesulfonyl)imide

Chemical Property:

• Melting Point: 9.5℃ (acetone )
• Refractive Index: 1.4380 to 1.4420
• PSA: 107.86000
• Density: 1.44
• LogP: 8.27160

Purity/Quality:

98%,99%, ^*data from raw suppliers

Tributyl(2-methoxyethyl)phosphonium Bis(trifluoromethanesulfonyl)imide >95.0%(N) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tributyl(2-methoxyethyl)phosphonium Bis(trifluoromethanesulfonyl)imide

There total 2 articles about Tributyl(2-methoxyethyl)phosphonium Bis(trifluoromethanesulfonyl)imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(2-methoxyethyl)tributylphosphonium bromide + bis(trifluoromethane)sulfonimide lithium (90076-65-6) → 2-methoxyethyl-tributylphosphonium bis(trifluoromethylsulfonyl)imide (959698-44-3)

Guidance literature:

In ethanol; at 20 ℃; for 17h;

DOI:10.1016/j.tetlet.2007.09.010

Reference yield:

tributylphosphine (998-40-3) → 2-methoxyethyl-tributylphosphonium bis(trifluoromethylsulfonyl)imide (959698-44-3)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 22 h / 80 °C

2: ethanol / 17 h / 20 °C

In ethanol;

DOI:10.1002/hc.20696

upstream raw materials:

bis(trifluoromethane)sulfonimide lithium

tributylphosphine

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