Carbamic acid, [(4-cyanophenyl)methylene]-, methyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, [(4-cyanophenyl)methylene]-, methyl ester (9CI)
CAS No.:199604-25-6
Molecular Formula:C10H8N2O2
Molecular Weight:188.18
Hs Code.:
Mol file:199604-25-6.mol

Synonyms:Carbamic acid, [(4-cyanophenyl)methylene]-, methyl ester (9CI)

Suppliers and Price of Carbamic acid, [(4-cyanophenyl)methylene]-, methyl ester (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Carbamic acid, [(4-cyanophenyl)methylene]-, methyl ester (9CI)

Chemical Property:

Melting Point:177 °C (tetrahydrofuran)
Boiling Point:322.6±44.0 °C(Predicted)
PKA:-1.62±0.50(Predicted)
PSA：62.45000
Density:1.11±0.1 g/cm3(Predicted)
LogP:1.74358

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Carbamic acid, [(4-cyanophenyl)methylene]-, methyl ester (9CI)

There total 2 articles about Carbamic acid, [(4-cyanophenyl)methylene]-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 79-22-1
methyl chloroformate

: 199604-07-4
N-trimethylsilyl-4-cyanobenzaldimine

: 199604-25-6
N-methoxycarbonyl-4-cyanobenzaldimine

Guidance literature:: In chloroform; for 3h; Heating;
DOI:10.1002/chem.19970031019

Reference yield:

: 105-07-7
4-cyanobenzaldehyde

: 199604-25-6
N-methoxycarbonyl-4-cyanobenzaldimine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / BuLi / hexane; tetrahydrofuran / 1.) 0 deg C, 10 min, 2.) r.t., 1 h

2: 50 percent / CHCl₃ / 3 h / Heating

With n-butyllithium; In tetrahydrofuran; hexane; chloroform;
DOI:10.1002/chem.19970031019