9β,10β-Bis(4-bromophenyl)-9,10-dihydroanthracene-9α,10α-diol

Base Information

• Chemical Name: 9β,10β-Bis(4-bromophenyl)-9,10-dihydroanthracene-9α,10α-diol
• CAS No.: 55517-98-1
• Molecular Formula: C₂₆H₁₈Br₂O₂
• Molecular Weight: 522.236
• Mol file: 55517-98-1.mol

Synonyms:9,10-Bis(4-bromophenyl)-9,10-dihydro-9α,10α-anthracenediol;9β,10β-Bis(4-bromophenyl)-9,10-dihydroanthracene-9α,10α-diol

Chemical Property of 9β,10β-Bis(4-bromophenyl)-9,10-dihydroanthracene-9α,10α-diol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9β,10β-Bis(4-bromophenyl)-9,10-dihydroanthracene-9α,10α-diol

There total 3 articles about 9β,10β-Bis(4-bromophenyl)-9,10-dihydroanthracene-9α,10α-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1.4-dibromobenzene (106-37-6) + 9,10-phenanthrenequinone (84-65-1) → 9,10-bis-(4-bromo-phenyl)-9,10-dihydro-anthracene-9,10-diol (55517-98-1)

Guidance literature:

1.4-dibromobenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.75h;

9,10-phenanthrenequinone; In tetrahydrofuran; hexane; at -78 ℃; for 2.5h;

DOI:10.1021/acs.joc.7b02590

Reference yield:

9,10-phenanthrenequinone (84-65-1) → 9,10-bis-(4-bromo-phenyl)-9,10-dihydro-anthracene-9,10-diol (55517-98-1)

Guidance literature:

With diethyl ether;

Reference yield:

9,10-phenanthrenequinone (84-65-1) → 9,10-bis-(4-bromo-phenyl)-9,10-dihydro-anthracene-9,10-diol (55517-98-1)

Guidance literature:

With toluene; Erhitzen des vom Aether befreiten Reaktionsgemisches auf 110grad;

upstream raw materials:

9,10-phenanthrenequinone

1.4-dibromobenzene

Downstream raw materials:

9,10‐bis(4‐bromophenyl)anthracene

4,4’-(anthracene-9,10-diyl)dibenzoic acid