tert-Butyl (10-hydroxydecyl)carbamate

Base Information

Chemical Name:tert-Butyl (10-hydroxydecyl)carbamate
CAS No.:173606-54-7
Molecular Formula:C15H31NO3
Molecular Weight:273.416
Hs Code.:
DSSTox Substance ID:DTXSID60402384
Wikidata:Q82205786
Mol file:173606-54-7.mol

Synonyms:173606-54-7;10-(t-Boc-amino)-1-decanol;tert-Butyl (10-hydroxydecyl)carbamate;Tert-butyl N-(10-hydroxydecyl)carbamate;N-Boc-10-aminodecan-1-ol;10-(Boc-amino)-1-decanol;SCHEMBL7908254;DTXSID60402384;MFCD02094530;AT29760;BS-51251;SY293516;CS-0120628;FT-0663434;Carbamic acid, N-(10-hydroxydecyl)-, 1,1-dimethylethyl ester

Suppliers and Price of tert-Butyl (10-hydroxydecyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
10-(t-Boc-amino)-1-decanol
500mg
$ 925.00

Medical Isotopes, Inc.
10-(t-Boc-amino)-1-decanol
0.5 g
$ 1640.00

Medical Isotopes, Inc.
10-(t-Boc-amino)-1-decanol
100 mg
$ 830.00

Biosynth Carbosynth
10-(t-Boc-amino)-1-decanol
500 mg
$ 600.00

Biosynth Carbosynth
10-(t-Boc-amino)-1-decanol
250 mg
$ 500.00

Biosynth Carbosynth
10-(t-Boc-amino)-1-decanol
100 mg
$ 400.00

Biosynth Carbosynth
10-(t-Boc-amino)-1-decanol
1 g
$ 900.00

Biosynth Carbosynth
10-(t-Boc-amino)-1-decanol
2 g
$ 1200.00

American Custom Chemicals Corporation
10-(T-BOC-AMINO)-1-DECANOL 95.00%
100MG
$ 716.10

American Custom Chemicals Corporation
10-(T-BOC-AMINO)-1-DECANOL 95.00%
1G
$ 1686.30

Total 6 raw suppliers

Chemical Property of tert-Butyl (10-hydroxydecyl)carbamate

Chemical Property:

Vapor Pressure:1.35E-07mmHg at 25°C
Melting Point:48-54°C
Boiling Point:387.2°C at 760 mmHg
Flash Point:188°C
PSA：62.05000
Density:0.956g/cm³
LogP:3.82860
Storage Temp.:-20°C Freezer
Solubility.:Dichloromethane, Chloroform (Slightly), Ether, Ethyl Acetate, Methanol (Slightly
XLogP3:3.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:12
Exact Mass:273.23039385
Heavy Atom Count:19
Complexity:224

Purity/Quality:

99% ^*data from raw suppliers

10-(t-Boc-amino)-1-decanol ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NCCCCCCCCCCO

Technology Process of tert-Butyl (10-hydroxydecyl)carbamate

There total 13 articles about tert-Butyl (10-hydroxydecyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 23160-46-5
10-amino-1-decanol

: 24424-99-5
di-tert-butyl dicarbonate

: 173606-54-7
(10-hydroxydecyl)carbamic acid tert-butyl ester

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2010.09.109

Reference yield: 76.0%

: 173606-53-6
tert-butyl (10-((tert-butyldimethylsilyl)oxy)decyl)carbamate

: 173606-54-7
(10-hydroxydecyl)carbamic acid tert-butyl ester

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/0040-4039(95)01977-P

Reference yield:

: 55362-80-6
9-bromononan-1-ol

: 173606-54-7
(10-hydroxydecyl)carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / Et₃N, DMAP / CH₂Cl₂

2: 68 percent / dimethylsulfoxide

3: 80 percent / LiAlH₄

4: 92 percent / Et₃N / CH₂Cl₂

5: 76 percent / nBu₄NF / tetrahydrofuran

With dmap; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/0040-4039(95)01977-P