3-Furancarboxylic acid, 5-(4-bromophenyl)-2-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-, ethyl ester

Base Information

Chemical Name:3-Furancarboxylic acid, 5-(4-bromophenyl)-2-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-, ethyl ester
CAS No.:960521-59-9
Molecular Formula:C24H30BrNO4
Molecular Weight:476.411
Hs Code.:
Mol file:960521-59-9.mol

Synonyms:3-Furancarboxylic acid, 5-(4-bromophenyl)-2-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-, ethyl ester

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Chemical Property of 3-Furancarboxylic acid, 5-(4-bromophenyl)-2-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-, ethyl ester

Chemical Property:

PSA：59.75000
LogP:6.45350

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Furancarboxylic acid, 5-(4-bromophenyl)-2-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-, ethyl ester

There total 1 articles about 3-Furancarboxylic acid, 5-(4-bromophenyl)-2-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 960521-58-8
ethyl 5-(4-bromophenyl)-2-[(1-methylethyl)amino]-3-furancarboxylate

: 55930-23-9
trans-4-methylcyclohexanecarbonyl chloride

: 960521-59-9
ethyl 5-(4-bromophenyl)-2-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-3-furancarboxylate

Guidance literature:: ethyl 5-(4-bromophenyl)-2-[(1-methylethyl)amino]-3-furancarboxylate; trans-4-methylcyclohexanecarbonyl chloride; In 1,2-dichloro-ethane; for 48h; Heating / reflux; Under notrogen;

trans-4-methylcyclohexanecarbonyl chloride; In 1,2-dichloro-ethane; for 24h;

With sodium hydrogencarbonate; In water; 1,2-dichloro-ethane;

Reference yield:

: 960521-59-9
ethyl 5-(4-bromophenyl)-2-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-3-furancarboxylate

: 960522-03-6
5-(4-bromophenyl)-2-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-3-furancarboxylic acid

Guidance literature:: ethyl 5-(4-bromophenyl)-2-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-3-furancarboxylate; With lithium hydroxide; In tetrahydrofuran; ethanol; water; at 20 ℃; for 16h;

With hydrogenchloride; In tetrahydrofuran; ethanol; water;

Reference yield:

: 960521-59-9
ethyl 5-(4-bromophenyl)-2-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-3-furancarboxylate

: 1066-54-2
trimethylsilylacetylene

: 960521-60-2
ethyl 2-[[(trans-4-methylcyclohexyl)carbonyl](1-methylethyl)amino]-5-{4-[2-(trimethylsilyl)ethynyl]phenyl}-3-furancarboxylate

Guidance literature:: With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; at 55 ℃; for 2h;