4-METHOXY-2-NITROPHENYL ACETALDEHYDE

Base Information

Chemical Name:4-METHOXY-2-NITROPHENYL ACETALDEHYDE
CAS No.:69111-92-8
Molecular Formula:C9H9NO4
Molecular Weight:195.175
Hs Code.:
Mol file:69111-92-8.mol

Synonyms:4-METHOXY-2-NITROPHENYL ACETALDEHYDE

Suppliers and Price of 4-METHOXY-2-NITROPHENYL ACETALDEHYDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Methoxy-2-nitrophenylacetaldehyde
1mg
$ 45.00

American Custom Chemicals Corporation
2-(4-METHOXY-2-NITROPHENYL)ACETALDEHYDE 95.00%
5MG
$ 502.84

Total 2 raw suppliers

Chemical Property of 4-METHOXY-2-NITROPHENYL ACETALDEHYDE

Chemical Property:

PSA：72.12000
LogP:1.86800

Purity/Quality:

98% ^*data from raw suppliers

4-Methoxy-2-nitrophenylacetaldehyde ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-METHOXY-2-NITROPHENYL ACETALDEHYDE

There total 5 articles about 4-METHOXY-2-NITROPHENYL ACETALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 109-92-2,25104-37-4
ethyl vinyl ether

: 96-96-8
4-methoxy-2-nitroaniline

: 69111-92-8
2-(4-methoxy-2-nitrophenyl)acetaldehyde

Guidance literature:: 4-methoxy-2-nitroaniline; With hydrogenchloride; In water; acetone;

With sodium nitrite; In water; acetone; for 0.05h; Sonication;

ethyl vinyl ether; Further stages;
DOI:10.1021/ja305660a

Reference yield:

: 1050514-02-7
2-(4-methoxy-2-nitrophenyl)ethanol

: 69111-92-8
2-(4-methoxy-2-nitrophenyl)acetaldehyde

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1002/jhet.1982

Reference yield:

: 96-96-8
4-methoxy-2-nitroaniline

: 69111-92-8
2-(4-methoxy-2-nitrophenyl)acetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: conc. aq. HCl, NaNO₂ / H₂O / 0.25 h / -5 - 2 °C

2: LiCl, CuCl*2H₂O / H₂O; acetone / 1.) 2 h, 3 to 10 deg C, 2.) 2 h, 10 deg C to room temp., 3.) 2 h, room temp.

With hydrogenchloride; lithium chloride; sodium nitrite; In water; acetone;
DOI:10.1021/jo00160a026