tert-butyl 3-hydroxyphenethylmethylcarbamate

Base Information

Chemical Name:tert-butyl 3-hydroxyphenethylmethylcarbamate
CAS No.:132513-31-6
Molecular Formula:C₁₄H₂₁NO₃
Molecular Weight:251.326
Hs Code.:

Synonyms:tert-butyl 3-hydroxyphenethylmethylcarbamate

Suppliers and Price of tert-butyl 3-hydroxyphenethylmethylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of tert-butyl 3-hydroxyphenethylmethylcarbamate

Chemical Property:

Purity/Quality:: 99% ，98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl 3-hydroxyphenethylmethylcarbamate

There total 4 articles about tert-butyl 3-hydroxyphenethylmethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 51674-33-0
2-(3-Hydroxyphenyl)-methylaminoethane

: 132513-31-6
tert-butyl (3-hydroxyphenethyl)(methyl)carbamate

Guidance literature:: With sodium hydrogencarbonate; In 1,4-dioxane; at 20 ℃; for 4h;
DOI:10.1021/jm020120c

Reference yield:

: 1093938-84-1
tert-butyl 3-methoxyphenethyl(methyl)carbamate

: 132513-31-6
tert-butyl (3-hydroxyphenethyl)(methyl)carbamate

Guidance literature:: tert-butyl 3-methoxyphenethyl(methyl)carbamate; With hydrogen bromide; In water; at 110 ℃; for 16h;

With sodium hydroxide; In water; at 0 ℃;

With di-tert-butyl dicarbonate; In 1,4-dioxane; water; at 22 ℃; for 2h;

Reference yield:

: 33543-62-3
2-(3-methoxyphenyl)-N-methylethan-1-amine

: 132513-31-6
tert-butyl (3-hydroxyphenethyl)(methyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; hydrogen bromide / water / 4 h / Reflux

2: triethylamine / tetrahydrofuran / 18 h / 20 °C

With hydrogen bromide; acetic acid; triethylamine; In tetrahydrofuran; water;
DOI:10.1021/acs.jmedchem.5b01330