10,11-dihydro-5H-dibenzo[b,f]azepin-10-o

Base Information

• Chemical Name: 10,11-dihydro-5H-dibenzo[b,f]azepin-10-o
• CAS No.: 4014-77-1
• Molecular Formula: C14H13NO
• Molecular Weight: 211.263
• Hs Code.: 2933990090
• Mol file: 4014-77-1.mol

Synonyms:10,11-dihydro-5H-dibenzo[b,f]azepin-10-o;10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol

Chemical Property of 10,11-dihydro-5H-dibenzo[b,f]azepin-10-o

Chemical Property:

• PSA: 32.26000
• LogP: 3.15770

Purity/Quality:

97% ^*data from raw suppliers

10,11-Dihydro-5H-dibenzo[b,f]azepin-10-ol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 10,11-dihydro-5H-dibenzo[b,f]azepin-10-o

There total 3 articles about 10,11-dihydro-5H-dibenzo[b,f]azepin-10-o which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

10,11-dihydro-5H-dibenzo[b,f]azepin-10-one (21737-58-6) → 10,11-dihydro-5H-dibenzo[b,f]azepin-10-ol?? (4014-77-1)

Guidance literature:

With sodium tetrahydroborate; In methanol; water; at 45 ℃; for 1h;

DOI:10.1016/j.tetlet.2013.03.089

Reference yield:

10-methoxy-5H-dibenzo[b,f]azepine (4698-11-7) → 10,11-dihydro-5H-dibenzo[b,f]azepin-10-ol?? (4014-77-1)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride / isopropyl alcohol; water / 25 - 65 °C

2: sodium tetrahydroborate / water; methanol / 1 h / 45 °C

With hydrogenchloride; sodium tetrahydroborate; In methanol; water; isopropyl alcohol;

DOI:10.1016/j.tetlet.2013.03.089

Reference yield:

→ 10,11-dihydro-5H-dibenzo[b,f]azepin-10-ol?? (4014-77-1)

Guidance literature:

(5H)-10,11-Dihydro-10-dibenzazepinon, NaBH4;

DOI:10.1021/jm00299a046

upstream raw materials:

10-methoxy-5H-dibenzo[b,f]azepine

10,11-dihydro-5H-dibenzo[b,f]azepin-10-one

Downstream raw materials:

dibenzoazepine

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