3-Bromo-2,6-dichloroaniline

Base Information

• Chemical Name: 3-Bromo-2,6-dichloroaniline
• CAS No.: 943830-82-8
• Molecular Formula: C₆H₄BrCl₂N
• Molecular Weight: 240.914
• Hs Code.: 2921420090
• DSSTox Substance ID: DTXSID60600944
• Wikidata: Q82497278
• Mol file: 943830-82-8.mol

Synonyms:3-BROMO-2,6-DICHLOROANILINE;943830-82-8;3-Bromo-2,6-dichloro-aniline;MFCD18432769;SCHEMBL3836844;DTXSID60600944;CS1944;Benzenamine, 3-bromo-2,6-dichloro-;AKOS015949283;PB16810;AS-46563;DA-24069;CS-0051487;J-511836

Chemical Property of 3-Bromo-2,6-dichloroaniline

Chemical Property:

• PSA: 26.02000
• LogP: 3.91930
• XLogP3: 3.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 238.89042
• Heavy Atom Count: 10
• Complexity: 122

Purity/Quality:

98%,99%, ^*data from raw suppliers

3-Bromo-2,6-dichloroaniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C(=C1Cl)N)Cl)Br

Technology Process of 3-Bromo-2,6-dichloroaniline

There total 3 articles about 3-Bromo-2,6-dichloroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-bromo-2,4-dichloro-3-nitrobenzene → 3-Bromo-2,6-dichloroaniline (943830-82-8)

Guidance literature:

With iron; ammonium chloride; In methanol; at 80 ℃; for 4h;

DOI:10.1039/d1ob01457a

Reference yield:

2,6-dichloronitrobenzene (601-88-7) → 3-Bromo-2,6-dichloroaniline (943830-82-8)

Guidance literature:

Multi-step reaction with 2 steps

1: N-Bromosuccinimide; sulfuric acid / 16 h / 60 °C / Inert atmosphere

2: iron; ammonium chloride / methanol / 4 h / 80 °C

With N-Bromosuccinimide; sulfuric acid; iron; ammonium chloride; In methanol;

DOI:10.1039/d1ob01457a

Reference yield:

→ 3-Bromo-2,6-dichloroaniline (943830-82-8)

Guidance literature:

upstream raw materials:

2,6-dichloronitrobenzene

Refernces

• 1、 -. "6-(Poly-substituted aryl)-4-aminopicolinates and their use as herbicides". Page/Page column 12. . Retrieved 2008/06/13.