3-Allyl-2-hydroxy-5-nitrobenzaldehyde

Base Information

Chemical Name:3-Allyl-2-hydroxy-5-nitrobenzaldehyde
CAS No.:22037-27-0
Molecular Formula:C₁₀H₉NO₄
Molecular Weight:207.186
Hs Code.:
Mol file:22037-27-0.mol

Synonyms:3-Allyl-2-hydroxy-5-nitrobenzaldehyde

Suppliers and Price of 3-Allyl-2-hydroxy-5-nitrobenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
3-Allyl-2-hydroxy-5-nitrobenzaldehyde 95+%
1g
$ 608.00

Alichem
3-Allyl-2-hydroxy-5-nitrobenzaldehyde
1g
$ 509.85

Total 4 raw suppliers

Chemical Property of 3-Allyl-2-hydroxy-5-nitrobenzaldehyde

Chemical Property:

PSA：83.12000
LogP:2.36460

Purity/Quality:

99% ^*data from raw suppliers

3-Allyl-2-hydroxy-5-nitrobenzaldehyde 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Allyl-2-hydroxy-5-nitrobenzaldehyde

There total 4 articles about 3-Allyl-2-hydroxy-5-nitrobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 96601-09-1
5-nitro-2-(prop-2-en-1-yloxy)benzaldehyde

: 22037-27-0
3-allyl-5-nitrosalicylaldehyde

Guidance literature:: at 200 ℃; for 4h;
DOI:10.1002/chem.201200859

Reference yield:

: 24019-66-7
3-allylsalicylaldehyde

: 22037-27-0
3-allyl-5-nitrosalicylaldehyde

Guidance literature:: durch Nitrierung;
DOI:10.1021/ja01530a021

Reference yield:

: 97-51-8
5-Nitrosalicylaldehyde

: 22037-27-0
3-allyl-5-nitrosalicylaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: tetra-(n-butyl)ammonium iodide; potassium carbonate / acetonitrile / 6 h / Reflux

2: 4 h / 200 °C

With tetra-(n-butyl)ammonium iodide; potassium carbonate; In acetonitrile; 2: |Claisen Rearrangement;
DOI:10.1002/chem.201200859