4-Methoxybiphenyl-3-carboxylic acid

Base Information

• Chemical Name: 4-Methoxybiphenyl-3-carboxylic acid
• CAS No.: 107410-07-1
• Molecular Formula: C14H12O3
• Molecular Weight: 228.247
• Nikkaji Number: J2.176.053F

Synonyms:4-methoxybiphenyl-3-carboxylic acid;107410-07-1;2-Methoxy-5-phenylbenzoic Acid;2-Methoxy-5-phenyl-benzoic acid;4-METHOXY-[1,1'-BIPHENYL]-3-CARBOXYLIC ACID;MFCD06203601;SCHEMBL3996761;NRUOSOAWSBPNPB-UHFFFAOYSA-N;BBL018911;STL195600;AKOS005151265;NS-02901;CS-0369112;E74964

Chemical Property of 4-Methoxybiphenyl-3-carboxylic acid

Chemical Property:

• PSA: 46.53000
• LogP: 3.06040
• XLogP3: 3.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 228.078644241
• Heavy Atom Count: 17
• Complexity: 258

Purity/Quality:

97% ^*data from raw suppliers

4-Methoxybiphenyl-3-carboxylicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C=C(C=C1)C2=CC=CC=C2)C(=O)O
• Uses: 4-Methoxybiphenyl-3-carboxylic Acid is a useful reagent for the preparation of polymyxin derivatives as antibacterial agents.

Technology Process of 4-Methoxybiphenyl-3-carboxylic acid

There total 12 articles about 4-Methoxybiphenyl-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

methyl 4-methoxy-[1,1'-biphenyl]-3-carboxylate (17504-10-8) → 2-methoxy-5-phenylbenzoic acid (107410-07-1)

Guidance literature:

With water; potassium hydroxide; In ethanol; for 3h; Reflux;

Reference yield:

2-methoxy-5-phenylacetophenone (412027-31-7) → 2-methoxy-5-phenylbenzoic acid (107410-07-1)

Guidance literature:

With potassium hydroxide; bromine; In 1,4-dioxane; at 20 ℃;

DOI:10.1016/j.bmc.2007.07.010

Reference yield:

sodium tetraphenyl borate (143-66-8) + 5-bromo-2-methoxybenzoic acid (2476-35-9) → 2-methoxy-5-phenylbenzoic acid (107410-07-1)

Guidance literature:

With sodium carbonate; palladium on activated charcoal; In water; for 1h; Heating;

DOI:10.1016/j.tetlet.2005.04.022

upstream raw materials:

4-(4-methoxy-biphenyl-3-yl)-4-oxo-butyric acid

4-methoxy-3-methyl-1,1'-biphenyl

sodium tetraphenyl borate

5-bromo-2-methoxybenzoic acid

Downstream raw materials:

4-methoxylbiphenyl

4-hydroxybiphenyl-3-carboxylic acid

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