2-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepine

Base Information

• Chemical Name: 2-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepine
• CAS No.: 10004-03-2
• Molecular Formula: C15H15NO
• Molecular Weight: 225.2857
• Hs Code.: 2934999090
• Mol file: 10004-03-2.mol

Synonyms:2-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepine

Chemical Property of 2-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepine

Chemical Property:

• PSA: 21.26000
• LogP: 3.23870

Purity/Quality:

98%min ^*data from raw suppliers

2-Phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepine

There total 3 articles about 2-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-phenyl-3,4-dihydrobenzo[f ][1,4]oxazepin-5(2H)-one (22217-08-9) → 2-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepine (10004-03-2)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 1.5h; Reflux;

DOI:10.3762/bjoc.10.272

Reference yield:

Flavanone (487-26-3) → 2-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepine (10004-03-2)

Guidance literature:

Multi-step reaction with 2 steps

1: trifluoroacetic acid; sodium azide / 6 h

2: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / Reflux

With lithium aluminium tetrahydride; sodium azide; trifluoroacetic acid; In tetrahydrofuran;

DOI:10.3762/bjoc.10.272

Reference yield:

→ 2-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepine (10004-03-2)

Guidance literature:

α-Phenyl-α-(2-carbamoylphenoxy)essigsaeure, 1) Δ mit PhCl, AcCl, 2) LiAlH4/ THF;

upstream raw materials:

2-phenyl-3,4-dihydrobenzo[f ][1,4]oxazepin-5(2H)-one

Flavanone

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