Technology Process of 3-Cyclohexene-1-carboxylicacid,2-hydroxy-,methylester,(1R-cis)-(9CI)
There total 5 articles about 3-Cyclohexene-1-carboxylicacid,2-hydroxy-,methylester,(1R-cis)-(9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
molybdenum hexacarbonyl; boric acid;
In
methanol; acetonitrile;
for 3h;
Heating;
DOI:10.1021/ja973081g
- Guidance literature:
-
Multi-step reaction with 5 steps
1: bis(η3-allyl-μ-chloropalladium(II)); (-)-(1,2)-bis<(diphenylphosphino)benzamido>cyclohexane; sodium hydrogencarbonate / tetrahydrofuran / 1 h
2: (dibenzylideneacetone)palladium; triphenylphosphine / tetrahydrofuran / 4 h / 60 °C
3: tin(ll) chloride / acetonitrile / 24 h / Ambient temperature
4: potassium carbonate / 1 h / Heating
5: molybdenum hexacarbonyl; boric acid / methanol; acetonitrile / 3 h / Heating
With
(dibenzylideneacetone)palladium; bis(η3-allyl-μ-chloropalladium(II)); (-)-(1,2)-bis<(diphenylphosphino)benzamido>cyclohexane; molybdenum hexacarbonyl; boric acid; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine; tin(ll) chloride;
In
tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/ja973081g
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / 1 h / Heating
2: molybdenum hexacarbonyl; boric acid / methanol; acetonitrile / 3 h / Heating
With
molybdenum hexacarbonyl; boric acid; potassium carbonate;
In
methanol; acetonitrile;
DOI:10.1021/ja973081g
