2-(4-Chloro-3,5-dimethylphenoxy)acetohydrazide

Base Information

• Chemical Name: 2-(4-Chloro-3,5-dimethylphenoxy)acetohydrazide
• CAS No.: 156867-62-8
• Molecular Formula: C₁₀H₁₃ClN₂O₂
• Molecular Weight: 228.678
• Hs Code.: 2928000090
• DSSTox Substance ID: DTXSID90351139
• Wikidata: Q82127312
• ChEMBL ID: CHEMBL4466083
• Mol file: 156867-62-8.mol

Synonyms:2-(4-chloro-3,5-dimethylphenoxy)acetohydrazide;156867-62-8;Cambridge id 5365951;Oprea1_432189;CHEMBL4466083;SCHEMBL11876050;DTXSID90351139;BDBM163685;BBL015540;MFCD00705188;STK093523;AKOS000295707;SB86239;VS-04964;CS-0279918;EN300-227916;AB00083178-01;SR-01000207215;SR-01000207215-1;3-AMINO-3-[5-(2,4-DICHLOROPHENYL)-FURAN-2-YL]-PROPIONICACID;2‐(4‐Chloro‐3,5‐dimethylphenoxy)acetohydrazide (0159)

Chemical Property of 2-(4-Chloro-3,5-dimethylphenoxy)acetohydrazide

Chemical Property:

• Vapor Pressure: 3.04E-08mmHg at 25°C
• Boiling Point: 448.7°C at 760 mmHg
• PKA: 12.11±0.35(Predicted)
• Flash Point: 225.2°C
• PSA: 64.35000
• Density: 1.242g/cm³
• LogP: 2.41670
• XLogP3: 1.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 228.0665554
• Heavy Atom Count: 15
• Complexity: 214

Purity/Quality:

98%min ^*data from raw suppliers

2-(4-Chloro-3,5-dimethylphenoxy)acetohydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=CC(=C1Cl)C)OCC(=O)NN

Technology Process of 2-(4-Chloro-3,5-dimethylphenoxy)acetohydrazide

There total 3 articles about 2-(4-Chloro-3,5-dimethylphenoxy)acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

ethyl 2-(4-chloro-3,5-dimethylphenoxy)acetate → 2-(4-chloro-3,5-dimethylphenoxy)acetohydrazide (156867-62-8)

Guidance literature:

With hydrazine hydrate; In ethanol; for 6h; Reflux;

Reference yield:

4-Chloro-3,5-dimethylphenol (88-04-0) → 2-(4-chloro-3,5-dimethylphenoxy)acetohydrazide (156867-62-8)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide

2: sulfuric acid

3: hydrazine

With sulfuric acid; sodium hydroxide; hydrazine;

Reference yield:

(4-chloro-3,5-dimethylphenoxy)acetic acid (19545-95-0) → 2-(4-chloro-3,5-dimethylphenoxy)acetohydrazide (156867-62-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid

2: hydrazine

With sulfuric acid; hydrazine;

upstream raw materials:

4-Chloro-3,5-dimethylphenol

(4-chloro-3,5-dimethylphenoxy)acetic acid

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