(5S,6S)-dihydroxy-7-(mesitylene-*sulfonyloxy)hept

Base Information

Chemical Name:(5S,6S)-dihydroxy-7-(mesitylene-*sulfonyloxy)hept
CAS No.:79308-42-2
Molecular Formula:C₁₈H₂₈O₇S
Molecular Weight:388.482
Hs Code.:

Synonyms:(5S,6S)-DIHYDROXY-7-(MESITYLENE-*SULFONY LOXY)HEPTAN;(5S,6S)-dihydroxy-7-(mesitylene-*sulfonyloxy)hept;dihydroxy-7-(mesitylenesulfonyoxy)heptanoic acid, ethyl

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Chemical Property of (5S,6S)-dihydroxy-7-(mesitylene-*sulfonyloxy)hept

Chemical Property:

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Technology Process of (5S,6S)-dihydroxy-7-(mesitylene-*sulfonyloxy)hept

There total 3 articles about (5S,6S)-dihydroxy-7-(mesitylene-*sulfonyloxy)hept which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 773-64-8
2-mesitylenesulphonyl chloride

: 79308-41-1
(5S,6R)-5,6,7-Trihydroxy-heptanoic acid ethyl ester

: 79308-42-2
(5S,6R)-5,6-Dihydroxy-7-(2,4,6-trimethyl-benzenesulfonyloxy)-heptanoic acid ethyl ester

Guidance literature:: In pyridine; at 0 ℃;
DOI:10.1016/S0040-4039(01)90545-3

Reference yield:

: 22900-10-3,35536-75-5,36792-85-5,113890-34-9,113890-37-2,133813-23-7
2-deoxy-D-ribose

: 79308-42-2
(5S,6R)-5,6-Dihydroxy-7-(2,4,6-trimethyl-benzenesulfonyloxy)-heptanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / tetrahydrofuran / 6 h / Heating

2: 80 percent / 10percent Pd/C

3: 57 percent / pyridine / 0 °C

With palladium on activated charcoal; In tetrahydrofuran; pyridine;
DOI:10.1016/S0040-4039(01)90545-3

Reference yield:

: 79308-40-0
ethyl 2,3,4-trideoxy-D-ribo-hept-2-enoate

: 79308-42-2
(5S,6R)-5,6-Dihydroxy-7-(2,4,6-trimethyl-benzenesulfonyloxy)-heptanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 10percent Pd/C

2: 57 percent / pyridine / 0 °C

With palladium on activated charcoal; In pyridine;
DOI:10.1016/S0040-4039(01)90545-3