3-Hydroxy-3-(4-chlorophenyl)propenedithioic acid

Base Information

Chemical Name:3-Hydroxy-3-(4-chlorophenyl)propenedithioic acid
CAS No.:41467-12-3
Molecular Formula:C₉H₇ClOS₂
Molecular Weight:230.739
Hs Code.:
Mol file:41467-12-3.mol

Synonyms:3-(4-Chlorophenyl)-3-hydroxypropenedithioic acid;3-Hydroxy-3-(4-chlorophenyl)propenedithioic acid

Suppliers and Price of 3-Hydroxy-3-(4-chlorophenyl)propenedithioic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Hydroxy-3-(4-chlorophenyl)propenedithioic acid

Chemical Property:

Melting Point:99 - 101 °C
PSA：91.12000
LogP:3.49610

Purity/Quality:

Safty Information:

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Technology Process of 3-Hydroxy-3-(4-chlorophenyl)propenedithioic acid

There total 2 articles about 3-Hydroxy-3-(4-chlorophenyl)propenedithioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 104-88-1
4-chlorobenzaldehyde

: 41467-12-3
3-hydroxy-3-(p-chlorophenyl)-2-propenedithioic acid

Guidance literature:: 4-chlorobenzaldehyde; With sodium hydride; In tetrahydrofuran;

carbon disulfide; In tetrahydrofuran;
DOI:10.2147/IDR.S328132

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 99-91-2
para-chloroacetophenone

: 41467-12-3
3-hydroxy-3-(p-chlorophenyl)-2-propenedithioic acid

Guidance literature:: With sodium tert-pentoxide;

Reference yield: 54.0%

: 14494-93-0,23751-62-4,106678-35-7
bis(triphenylphosphino)copper(I) nitrate

: 41467-12-3
3-hydroxy-3-(p-chlorophenyl)-2-propenedithioic acid

: 828940-37-0
(3-hydroxy-3-(p-chlorophenyl)-2-propenedithioate-S,S')bis(triphenylphosphine-P)copper(I)

Guidance literature:: With NaOH; In dichloromethane; water; 1 equiv of complex in CH2Cl2 was added to an aq. soln. of dithioic acid and NaOH, the mixt. was stirred for 15 min; the organic layer was dried with Na2SO4, the solvent was distilled in vac., ethanol was added, ppt. was filtered out, dried under vac.; elem. anal.;
DOI:10.1021/ic0488132