3-Methoxy-5,5,8,8-tetraMethyl-5,6,7,8-tetrahydronaphthalen-2-aMine

Base Information

• Chemical Name: 3-Methoxy-5,5,8,8-tetraMethyl-5,6,7,8-tetrahydronaphthalen-2-aMine
• CAS No.: 457065-49-5
• Molecular Formula: C₁₅H₂₃NO
• Molecular Weight: 233.354
• Mol file: 457065-49-5.mol

Synonyms:3-Methoxy-5,5,8,8-tetraMethyl-5,6,7,8-tetrahydronaphthalen-2-aMine

Chemical Property of 3-Methoxy-5,5,8,8-tetraMethyl-5,6,7,8-tetrahydronaphthalen-2-aMine

Chemical Property:

• PSA: 35.25000
• LogP: 4.20760
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

97% ^*data from raw suppliers

3-Methoxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-amine 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3-Methoxy-5,5,8,8-tetraMethyl-5,6,7,8-tetrahydronaphthalen-2-aMine

There total 5 articles about 3-Methoxy-5,5,8,8-tetraMethyl-5,6,7,8-tetrahydronaphthalen-2-aMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

6-methoxy-1,1,4,4-tetramethyl-7-nitro-1,2,3,4-tetrahydro-naphthalene (457065-48-4) → 3-methoxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalen-2-ylamine (457065-49-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol;

DOI:10.1016/j.bmcl.2005.12.003

Reference yield:

5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-ol (22824-31-3) → 3-methoxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalen-2-ylamine (457065-49-5)

Guidance literature:

Multi-step reaction with 3 steps

1: HNO₃

2: K₂CO₃ / acetone

3: 100 percent / H₂ / Pd/C / ethanol

With hydrogen; nitric acid; potassium carbonate; palladium on activated charcoal; In ethanol; acetone;

DOI:10.1016/j.bmcl.2005.12.003

Reference yield:

5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-3-nitro-naphth-2-ol (122284-35-9) → 3-methoxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalen-2-ylamine (457065-49-5)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / acetone

2: 100 percent / H₂ / Pd/C / ethanol

With hydrogen; potassium carbonate; palladium on activated charcoal; In ethanol; acetone;

DOI:10.1016/j.bmcl.2005.12.003

upstream raw materials:

6-methoxy-1,1,4,4-tetramethyl-7-nitro-1,2,3,4-tetrahydro-naphthalene

2,5-dichloro-2,5-dimethyl hexane

5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-ol

5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-3-nitro-naphth-2-ol

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