1,3-DIMETHYL-BENZO[4,5]IMIDAZO[1,2-A]PYRIDINE-4-CARBOXYLIC ACID

Base Information

• Chemical Name: 1,3-DIMETHYL-BENZO[4,5]IMIDAZO[1,2-A]PYRIDINE-4-CARBOXYLIC ACID
• CAS No.: 10326-57-5
• Molecular Formula: C14H12N2O2
• Molecular Weight: 240.26
• Hs Code.: 2933990090
• Mol file: 10326-57-5.mol

Synonyms:AKOS BBS-00002690;AKOS BC-1832;1,3-DIMETHYL-BENZO[4,5]IMIDAZO[1,2-A]PYRIDINE-4-CARBOXYLIC ACID

Chemical Property of 1,3-DIMETHYL-BENZO[4,5]IMIDAZO[1,2-A]PYRIDINE-4-CARBOXYLIC ACID

Chemical Property:

• PSA: 54.60000
• LogP: 2.80250

Purity/Quality:

98%,99%, ^*data from raw suppliers

1,3-Dimethylbenzo[4,5]imidazo[1,2-a]pyridine-4-carboxylicAcid ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-DIMETHYL-BENZO[4,5]IMIDAZO[1,2-A]PYRIDINE-4-CARBOXYLIC ACID

There total 4 articles about 1,3-DIMETHYL-BENZO[4,5]IMIDAZO[1,2-A]PYRIDINE-4-CARBOXYLIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1,3-dimethyl-benzo[4,5]imidazo[1,2-a]pyridine-4-carbonitrile (16314-95-7) → 1,3-Dimethyl-4-carboxypyrido<1,2-a>benzimidazole (10326-57-5)

Guidance literature:

With sulfuric acid; In water; Reflux;

DOI:10.1007/s11030-016-9702-y

Reference yield:

1,2-diamino-benzene (95-54-5) → 1,3-Dimethyl-4-carboxypyrido<1,2-a>benzimidazole (10326-57-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 180 °C

2: perchloric acid / ethanol / Reflux

3: sulfuric acid / water / Reflux

With perchloric acid; sulfuric acid; In ethanol; water;

DOI:10.1007/s11030-016-9702-y

Reference yield:

1H-benzimidazol-2-acetonitrile (4414-88-4) → 1,3-Dimethyl-4-carboxypyrido<1,2-a>benzimidazole (10326-57-5)

Guidance literature:

Multi-step reaction with 2 steps

1: perchloric acid / ethanol / Reflux

2: sulfuric acid / water / Reflux

With perchloric acid; sulfuric acid; In ethanol; water;

DOI:10.1007/s11030-016-9702-y

upstream raw materials:

1,3-dimethyl-benzo[4,5]imidazo[1,2-a]pyridine-4-carbonitrile

1,2-diamino-benzene

1H-benzimidazol-2-acetonitrile

Downstream raw materials:

1,3-Dimethylpyrido<1,2-a>benzimidazole

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