2-Bromo-1-iodonaphthalene

Base Information

Chemical Name:2-Bromo-1-iodonaphthalene
CAS No.:676267-05-3
Molecular Formula:C10H6BrI
Molecular Weight:332.966
Hs Code.:
Mol file:676267-05-3.mol

Synonyms:2-Bromo-1-iodonaphthalene

Suppliers and Price of 2-Bromo-1-iodonaphthalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
2-Bromo-1-iodonaphthalene
1g
$ 1769.25

Alichem
2-Bromo-1-iodonaphthalene
500mg
$ 940.80

Alichem
2-Bromo-1-iodonaphthalene
250mg
$ 680.00

Total 11 raw suppliers

Chemical Property of 2-Bromo-1-iodonaphthalene

Chemical Property:

Melting Point:65 °C
Boiling Point:361.8±15.0 °C(Predicted)
PSA：0.00000
Density:2.057±0.06 g/cm3(Predicted)
LogP:4.20690

Purity/Quality:

97% ^*data from raw suppliers

2-Bromo-1-iodonaphthalene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Bromo-1-iodonaphthalene

There total 2 articles about 2-Bromo-1-iodonaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 771-14-2
2-bromonaphthalen-1-amine

: 676267-05-3
2-bromo-1-iodonaphthalene

Guidance literature:: 2-bromonaphthalen-1-amine; With hydrogenchloride; In water; at 20 ℃; for 0.333333h;

With sodium nitrite; In water; at 4 ℃; for 0.5h;

With potassium iodide; In water; at 20 - 60 ℃; for 1.75h;
DOI:10.1002/anie.201301739

Reference yield:

: 4185-62-0
2-bromo-1-nitronaphthalene

: 676267-05-3
2-bromo-1-iodonaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: iron; aqueous iron (II)-sulfate

2: aqueous H₂SO₄ / Diazotization_.Behandlung der Diazoniumsalz-Loesung mit KI

With sulfuric acid; iron; iron(II) sulfate;
DOI:10.1039/jr9440000538

Reference yield: 95.0%

: 38274-16-7
2-bromo-1-(trimethylsilylethynyl)benzene

: 676267-05-3
2-bromo-1-iodonaphthalene

: 2-bromo-1-[(2-bromophenyl)ethynyl]naphthalene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In water; benzene; at 43 ℃; for 18h; chemoselective reaction;
DOI:10.1002/anie.201301739