Benzoic acid, 4-[3-(acetyloxy)-2-methylpropyl]-, methyl ester, (R)- (9CI)

Base Information

Chemical Name:Benzoic acid, 4-[3-(acetyloxy)-2-methylpropyl]-, methyl ester, (R)- (9CI)
CAS No.:173065-76-4
Molecular Formula:C₁₄H₁₈O₄
Molecular Weight:250.295
Hs Code.:
Mol file:173065-76-4.mol

Synonyms:Benzoic acid, 4-[3-(acetyloxy)-2-methylpropyl]-, methyl ester, (R)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 4-[3-(acetyloxy)-2-methylpropyl]-, methyl ester, (R)- (9CI)

Chemical Property:

Boiling Point:349.4±35.0 °C(Predicted)
Density:1.088±0.06 g/cm3(Predicted)

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of Benzoic acid, 4-[3-(acetyloxy)-2-methylpropyl]-, methyl ester, (R)- (9CI)

There total 4 articles about Benzoic acid, 4-[3-(acetyloxy)-2-methylpropyl]-, methyl ester, (R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 108-24-7
acetic anhydride

: 170955-21-2
3-(4-methoxycarbonyl)phenyl-2-methyl-1-propanol

: 173065-76-4
3-(4-methoxycarbonyl)phenyl-2-methylprop-1-yl acetate

Guidance literature:: In pyridine; at 20 - 22 ℃; for 4.5h;
DOI:10.1007/BF00698514

Reference yield:

: 170955-20-1
3-(4-methoxycarbonyl)phenyl-2-methyl-2-propen-1-ol

: 173065-76-4
3-(4-methoxycarbonyl)phenyl-2-methylprop-1-yl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / H₂ / 5percent Pd/C / methanol / 48 h / Ambient temperature

2: 89 percent / pyridine / 4.5 h / 20 - 22 °C

With hydrogen; palladium on activated charcoal; In pyridine; methanol;
DOI:10.1007/BF00698514

Reference yield:

: 4-((E)-2-Methyl-3-oxo-propenyl)-benzoic acid methyl ester

: 173065-76-4
3-(4-methoxycarbonyl)phenyl-2-methylprop-1-yl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 2.05 g / NaBH₄ / methanol / 1.) -10 - -5 deg C, 4 h, 2.) overnight

2: 86 percent / H₂ / 5percent Pd/C / methanol / 48 h / Ambient temperature

3: 89 percent / pyridine / 4.5 h / 20 - 22 °C

With sodium tetrahydroborate; hydrogen; palladium on activated charcoal; In pyridine; methanol;
DOI:10.1007/BF00698514