2,4,6,8,9,10-Hexamethyl-2,4,6,8,9,10-hexaaza-1,3,5,7-tetraphosphatricyclo[3.3.1.13,7]decane1,3,5-trissulfide

Base Information

• Chemical Name: 2,4,6,8,9,10-Hexamethyl-2,4,6,8,9,10-hexaaza-1,3,5,7-tetraphosphatricyclo[3.3.1.13,7]decane1,3,5-trissulfide
• CAS No.: 38448-55-4
• Molecular Formula: C6H18N6P4S3
• Molecular Weight: 394.342
• Mol file: 38448-55-4.mol

Synonyms:2,4,6,8,9,10-Hexamethyl-2,4,6,8,9,10-hexaaza-1,3,5,7-tetraphosphatricyclo[3.3.1.13,7]decane1,3,5-trissulfide

Chemical Property of 2,4,6,8,9,10-Hexamethyl-2,4,6,8,9,10-hexaaza-1,3,5,7-tetraphosphatricyclo[3.3.1.13,7]decane1,3,5-trissulfide

Chemical Property:

• Melting Point: 174 °C
• PSA: 158.73000
• LogP: 4.09760

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4,6,8,9,10-Hexamethyl-2,4,6,8,9,10-hexaaza-1,3,5,7-tetraphosphatricyclo[3.3.1.13,7]decane1,3,5-trissulfide

There total 2 articles about 2,4,6,8,9,10-Hexamethyl-2,4,6,8,9,10-hexaaza-1,3,5,7-tetraphosphatricyclo[3.3.1.13,7]decane1,3,5-trissulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4,6,8,9,10-hexamethyl-2,4,6,8,9,10-hexaaza-1,3,5,7-tetraphophaadamantane (10369-17-2) → tetraphosphorus hexamethylimide trisulfide (38448-55-4)

Guidance literature:

With sulfur;

Reference yield:

→ tetraphosphorus hexamethylimide trisulfide (38448-55-4)

Guidance literature:

closo-Hexa-N-methylphosphorimid, Schwefel;

DOI:10.1021/ic50170a028

Reference yield: 75.0%

tetraphosphorus hexamethylimide trisulfide (38448-55-4) + tetracarbonyl nickel (13463-39-3,71564-36-8) → nickel tricarbonyl closo-hexa-N-methyltrithiophosphorimide (87636-60-0)

Guidance literature:

In neat (no solvent); with a vac. line, Ni-complex was condensed on to P4(NCH3)6S3 at liq. N2 temp., Ar was introduced, warmed to room temp., stirred for 1 h, the exess of Ni-complex was removed under a slight vac. at -20°C; recrystd. from pentane at -20°C; elem. anal.;

upstream raw materials:

2,4,6,8,9,10-hexamethyl-2,4,6,8,9,10-hexaaza-1,3,5,7-tetraphophaadamantane

Downstream raw materials:

nickel tricarbonyl closo-hexa-N-methyltrithiophosphorimide