3-(4-FLUORO-BENZYLOXY)-4-METHOXY-BENZALDEHYDE

Base Information

• Chemical Name: 3-(4-FLUORO-BENZYLOXY)-4-METHOXY-BENZALDEHYDE
• CAS No.: 351066-28-9
• Molecular Formula: C15H13FO3
• Molecular Weight: 260.265
• Mol file: 351066-28-9.mol

Synonyms:ASINEX-REAG BAS 13520216;ART-CHEM-BB B014189;CHEMBRDG-BB 3014189;AKOS B014189;3-(4-FLUORO-BENZYLOXY)-4-METHOXY-BENZALDEHYDE;TIMTEC-BB SBB009338;3-[(4-fluorobenzyl)oxy]-4-methoxybenzaldehyde(SALTDATA: FREE);3-[(4-fluorophenyl)methoxy]-4-methoxybenzaldehyde

Chemical Property of 3-(4-FLUORO-BENZYLOXY)-4-METHOXY-BENZALDEHYDE

Chemical Property:

• Vapor Pressure: 1.59E-06mmHg at 25°C
• Boiling Point: 397.4°C at 760 mmHg
• Flash Point: 187.4°C
• PSA: 35.53000
• Density: 1.216g/cm³
• LogP: 3.22580

Purity/Quality:

97% ^*data from raw suppliers

3-[(4-Fluorobenzyl)oxy]-4-methoxybenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(4-FLUORO-BENZYLOXY)-4-METHOXY-BENZALDEHYDE

There total 1 articles about 3-(4-FLUORO-BENZYLOXY)-4-METHOXY-BENZALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-methyl-acetamide (79-16-3) + C14H11FO3 (1257411-98-5) → 3-(4-fluorobenzyloxy)-4-methoxybenzaldehyde (351066-28-9)

Guidance literature:

With potassium carbonate; potassium iodide; In acetone; Reflux;

DOI:10.1016/j.ejmech.2017.02.032

Reference yield: 84.0%

3-(4-fluorobenzyloxy)-4-methoxybenzaldehyde (351066-28-9) + anthranilic acid amide (28144-70-9,88-68-6) → 2-(3-(4-fluorobenzyloxy)-4-methoxyphenyl)quinazolin-4(3H)-one

Guidance literature:

anthranilic acid amide; With sodium acetate; In N,N-dimethyl-formamide; for 0.166667h;

3-(4-fluorobenzyloxy)-4-methoxybenzaldehyde; With iodine; In N,N-dimethyl-formamide; at 70 - 80 ℃; for 24h;

DOI:10.1016/j.ejmech.2017.02.032

Reference yield:

C11H9F3N2O (931234-51-4) + 3-(4-fluorobenzyloxy)-4-methoxybenzaldehyde (351066-28-9) → C26H20F4N2O3 (1257412-10-4)

Guidance literature:

In water; Reflux;

DOI:10.1016/j.bmcl.2010.08.057

upstream raw materials:

N-methyl-acetamide

C₁₄H₁₁FO₃

Downstream raw materials:

C₂₆H₂₀F₄N₂O₃

C₂₆H₁₇F₇N₂O₃

C₃₁H₂₂F₄N₂O₃

C₂₅H₁₇F₄N₃O₅

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