(S)-3-AZIDO-2-(4-CHLOROBENZYL)PROPANAMIDE

Base Information

Chemical Name:(S)-3-AZIDO-2-(4-CHLOROBENZYL)PROPANAMIDE
CAS No.:916322-87-7
Molecular Formula:C₁₀H₁₁ClN₄O
Molecular Weight:238.677
Hs Code.:
Mol file:916322-87-7.mol

Synonyms:(S)-3-AZIDO-2-(4-CHLOROBENZYL)PROPANAMIDE;(S)-3-AZIDO-2-(4-BROMOBENZYL)PROPANAMIDE

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-AZIDO-2-(4-CHLOROBENZYL)PROPANAMIDE

Chemical Property:

Purity/Quality:

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Technology Process of (S)-3-AZIDO-2-(4-CHLOROBENZYL)PROPANAMIDE

There total 4 articles about (S)-3-AZIDO-2-(4-CHLOROBENZYL)PROPANAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2286-53-5
3-(4-chlorophenyl)-2-(hydroxymethyl)propanenitrile

: 916322-87-7
(R)-β-azido-α-(p-chlorophenylmethyl)propanamide

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; diisopropyl azodicarboxylate; hydrazoic acid / toluene; tetrahydrofuran / 0.02 h / 5 °C

2: Rhodococcus erythropolis AJ₂₇₀; potassium phosphate buffer / H₂O / 3.5 h / pH 7.0

With hydrogen azide; potassium phosphate buffer; di-isopropyl azodicarboxylate; Rhodococcus erythropolis AJ₂₇₀; triphenylphosphine; In tetrahydrofuran; water; toluene;
DOI:10.1016/j.tetasy.2006.08.021

Reference yield:

: 2286-53-5
3-(4-chlorophenyl)-2-(hydroxymethyl)propanenitrile

: 916322-87-7
(S)-β-azido-α-(p-chlorophenylmethyl)propanamide

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; diisopropyl azodicarboxylate; hydrazoic acid / toluene; tetrahydrofuran / 0.02 h / 5 °C

2: Rhodococcus erythropolis AJ₂₇₀; potassium phosphate buffer / H₂O / 3.5 h / pH 7.0

With hydrogen azide; potassium phosphate buffer; di-isopropyl azodicarboxylate; Rhodococcus erythropolis AJ₂₇₀; triphenylphosphine; In tetrahydrofuran; water; toluene;
DOI:10.1016/j.tetasy.2006.08.021

Reference yield:

: β-azido-α-(p-chlorophenylmethyl)propionitrile

: 916322-87-7
(R)-β-azido-α-(p-chlorophenylmethyl)propanamide

: 916322-87-7
(S)-β-azido-α-(p-chlorophenylmethyl)propanamide

: 916322-97-9
(R)-β-azido-α-(p-chlorophenylmethyl)propanoic acid

: 916322-97-9
(S)-β-azido-α-(p-chlorophenylmethyl)propanoic acid

Guidance literature:: With potassium phosphate buffer; Rhodococcus erythropolis AJ₂₇₀; In water; for 3.5h; pH=7.0; Title compound not separated from byproducts;
DOI:10.1016/j.tetasy.2006.08.021