benzyl 4-iodo-1H-pyrazole-1-carboxylate

Base Information

• Chemical Name: benzyl 4-iodo-1H-pyrazole-1-carboxylate
• CAS No.: 952338-83-9
• Molecular Formula: C11H9IN2O2
• Molecular Weight: 328.10583
• Mol file: 952338-83-9.mol

Synonyms:benzyl 4-iodo-1H-pyrazole-1-carboxylate

Chemical Property of benzyl 4-iodo-1H-pyrazole-1-carboxylate

Chemical Property:

• PSA: 44.12000
• LogP: 2.67260

Purity/Quality:

NLT 98% ^*data from raw suppliers

Benzyl4-iodo-1H-pyrazole-1-carboxylate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl 4-iodo-1H-pyrazole-1-carboxylate

There total 1 articles about benzyl 4-iodo-1H-pyrazole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-iodopyrazole (3469-69-0) + benzyl chloroformate (501-53-1,94274-21-2) → 4-iodopyrazole-1-carboxylic acid benzyl ester (952338-83-9)

Guidance literature:

With triethylamine; In toluene; at 0 ℃; for 1h;

Reference yield:

4-iodopyrazole-1-carboxylic acid benzyl ester (952338-83-9) + tri-n-butyl(vinyl)tin (7486-35-3) → 4-vinylpyrazole-1-carboxylic acid benzyl ester (952338-85-1)

Guidance literature:

tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tris-(o-tolyl)phosphine; In acetonitrile; at 80 ℃; for 3h;

upstream raw materials:

4-iodopyrazole

benzyl chloroformate

Downstream raw materials:

4-vinylpyrazole-1-carboxylic acid benzyl ester

Refernces